(S)-2-allyl-2-ethyl-N-benzoyl-δ-valerolactam

Base Information

Chemical Name:(S)-2-allyl-2-ethyl-N-benzoyl-δ-valerolactam
CAS No.:1354568-46-9
Molecular Formula:C₁₇H₂₁NO₂
Molecular Weight:271.359
Hs Code.:

Synonyms:(S)-2-allyl-2-ethyl-N-benzoyl-δ-valerolactam

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-allyl-2-ethyl-N-benzoyl-δ-valerolactam

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Technology Process of (S)-2-allyl-2-ethyl-N-benzoyl-δ-valerolactam

There total 4 articles about (S)-2-allyl-2-ethyl-N-benzoyl-δ-valerolactam which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.2%

: 1354568-46-9
(S)-2-allyl-2-ethyl-N-benzoyl-δ-valerolactam

Guidance literature:

Reference yield: 97.0%

: 1354568-15-2
C₁₈H₂₁NO₄

: 1354568-46-9
(S)-2-allyl-2-ethyl-N-benzoyl-δ-valerolactam

Guidance literature:: With (S)-2-(2-(bis(4-trifluoromethyl-phenyl)-phosphino))-5-(4-trifluoromethyl-phenyl)-4-tert-butyl-4,5-dihydro-oxazole; t r i s ( 4 , 4 ’-methoxydibenzylideneacetone)dipalladium(0); In toluene; at 40 ℃; optical yield given as %ee; enantioselective reaction;
DOI:10.1038/nchem.1222

Reference yield:

: 1354568-15-2
C₁₈H₂₁NO₄

: 1354568-46-9
(S)-2-allyl-2-ethyl-N-benzoyl-δ-valerolactam

: 2-allyl-2-ethyl-N-benzoyl-δ-valerolactam

Guidance literature:: With (S)-2-(2-(bis(4-trifluoromethyl-phenyl)-phosphino))-5-(4-trifluoromethyl-phenyl)-4-tert-butyl-4,5-dihydro-oxazole; palladium diacetate; at 60 ℃; for 16h; Overall yield = 77 %Chromat.; enantioselective reaction; Sealed tube; Inert atmosphere; Glovebox;
DOI:10.1002/adsc.201500253