Technology Process of (S,S)-N,N'-bis{1-[6-(4-bromophenoxy)hexyloxy]methyl-3-methylbutyl}perylene 3,4:9,10-perylenetetracarboxylicbisimide
There total 7 articles about (S,S)-N,N'-bis{1-[6-(4-bromophenoxy)hexyloxy]methyl-3-methylbutyl}perylene 3,4:9,10-perylenetetracarboxylicbisimide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 94 percent / toluene / 80 - 130 °C
2: 44 percent / potassium tert-butoxide / dimethylformamide / 42 h / 70 °C
3: hydrazine monohydrate / methanol / 42 h / Heating
4: 0.040 g / imidazole; zinc acetate / 1 h / 180 °C
With
1H-imidazole; potassium tert-butylate; zinc diacetate; hydrazine hydrate;
In
methanol; N,N-dimethyl-formamide; toluene;
2: Williamson etherification;
DOI:10.1021/ja034926t
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 91 percent / K2CO3; tetrabutylammonium bromide / acetone / 22 h / Heating
2: 75 percent / pyridine / 4 °C
3: 44 percent / potassium tert-butoxide / dimethylformamide / 42 h / 70 °C
4: hydrazine monohydrate / methanol / 42 h / Heating
5: 0.040 g / imidazole; zinc acetate / 1 h / 180 °C
With
pyridine; 1H-imidazole; potassium tert-butylate; zinc diacetate; tetrabutylammomium bromide; potassium carbonate; hydrazine hydrate;
In
methanol; N,N-dimethyl-formamide; acetone;
1: Williamson etherification / 3: Williamson etherification;
DOI:10.1021/ja034926t
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 91 percent / K2CO3; tetrabutylammonium bromide / acetone / 22 h / Heating
2: 75 percent / pyridine / 4 °C
3: 44 percent / potassium tert-butoxide / dimethylformamide / 42 h / 70 °C
4: hydrazine monohydrate / methanol / 42 h / Heating
5: 0.040 g / imidazole; zinc acetate / 1 h / 180 °C
With
pyridine; 1H-imidazole; potassium tert-butylate; zinc diacetate; tetrabutylammomium bromide; potassium carbonate; hydrazine hydrate;
In
methanol; N,N-dimethyl-formamide; acetone;
1: Williamson etherification / 3: Williamson etherification;
DOI:10.1021/ja034926t
