triethylammonium (1R,2R)-1-O-[3,4,6-tri-O-acetyl-C-(carboxymethyl N-tert-butyloxy-carbonyl-N-benzyloxyamide)-2-deoxy-β-D-glucopyranosyl]-cyclohexanediol 2-(n-octa-decyl phosphate)

Base Information

Chemical Name:triethylammonium (1R,2R)-1-O-[3,4,6-tri-O-acetyl-C-(carboxymethyl N-tert-butyloxy-carbonyl-N-benzyloxyamide)-2-deoxy-β-D-glucopyranosyl]-cyclohexanediol 2-(n-octa-decyl phosphate)
CAS No.:1364180-20-0
Molecular Formula:C₆H₁₅N*C₅₀H₈₂NO₁₆P
Molecular Weight:1085.36
Hs Code.:

triethylammonium (1R,2R)-1-O-[3,4,6-tri-O-acetyl-C-(carboxymethyl N-tert-butyloxy-carbonyl-N-benzyloxyamide)-2-deoxy-β-D-glucopyranosyl]-cyclohexanediol 2-(n-octa-decyl phosphate)

Synonyms:triethylammonium (1R,2R)-1-O-[3,4,6-tri-O-acetyl-C-(carboxymethyl N-tert-butyloxy-carbonyl-N-benzyloxyamide)-2-deoxy-β-D-glucopyranosyl]-cyclohexanediol 2-(n-octa-decyl phosphate)

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Chemical Property of triethylammonium (1R,2R)-1-O-[3,4,6-tri-O-acetyl-C-(carboxymethyl N-tert-butyloxy-carbonyl-N-benzyloxyamide)-2-deoxy-β-D-glucopyranosyl]-cyclohexanediol 2-(n-octa-decyl phosphate)

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Technology Process of triethylammonium (1R,2R)-1-O-[3,4,6-tri-O-acetyl-C-(carboxymethyl N-tert-butyloxy-carbonyl-N-benzyloxyamide)-2-deoxy-β-D-glucopyranosyl]-cyclohexanediol 2-(n-octa-decyl phosphate)

There total 5 articles about triethylammonium (1R,2R)-1-O-[3,4,6-tri-O-acetyl-C-(carboxymethyl N-tert-butyloxy-carbonyl-N-benzyloxyamide)-2-deoxy-β-D-glucopyranosyl]-cyclohexanediol 2-(n-octa-decyl phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₀H₈₂NO₁₅P

: 15715-58-9
triethylamine carbonate

: 1364180-20-0
triethylammonium (1R,2R)-1-O-[3,4,6-tri-O-acetyl-C-(carboxymethyl N-tert-butyloxy-carbonyl-N-benzyloxyamide)-2-deoxy-β-D-glucopyranosyl]-cyclohexanediol 2-(n-octa-decyl phosphate)

Guidance literature:: C₅₀H₈₂NO₁₅P; With iodine; In pyridine; water; at 20 ℃; for 0.75h; Inert atmosphere;

triethylamine carbonate; With sodium hydrogensulfite; In pyridine; dichloromethane; water; Inert atmosphere;
DOI:10.1111/j.1747-0285.2011.01300.x

Reference yield:

: 1363730-93-1
(1R,2R)-1-O-[3,4,6-tri-O-acetyl-2-C-(carboxymethyl N-tert-butyloxycarbonyl-N-benzyl-oxyamide)-2-deoxy-β-D-glucopyranosyl]-cyclohexanediol

: 1364180-20-0
triethylammonium (1R,2R)-1-O-[3,4,6-tri-O-acetyl-C-(carboxymethyl N-tert-butyloxy-carbonyl-N-benzyloxyamide)-2-deoxy-β-D-glucopyranosyl]-cyclohexanediol 2-(n-octa-decyl phosphate)

Guidance literature:: Multi-step reaction with 2 steps

1.1: pivaloyl chloride / pyridine / 2 h / Inert atmosphere

2.1: iodine / pyridine; water / 0.75 h / 20 °C / Inert atmosphere

2.2: Inert atmosphere

With iodine; pivaloyl chloride; In pyridine; water;
DOI:10.1111/j.1747-0285.2011.01300.x

Reference yield:

: n-octadecyl hydrogenphosphonate

: 1364180-20-0
triethylammonium (1R,2R)-1-O-[3,4,6-tri-O-acetyl-C-(carboxymethyl N-tert-butyloxy-carbonyl-N-benzyloxyamide)-2-deoxy-β-D-glucopyranosyl]-cyclohexanediol 2-(n-octa-decyl phosphate)

Guidance literature:: Multi-step reaction with 2 steps

1.1: pivaloyl chloride / pyridine / 2 h / Inert atmosphere

2.1: iodine / pyridine; water / 0.75 h / 20 °C / Inert atmosphere

2.2: Inert atmosphere

With iodine; pivaloyl chloride; In pyridine; water;
DOI:10.1111/j.1747-0285.2011.01300.x