WBr(CO)2((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2⁽¹⁺⁾*Br^(1-)=WBr(CO)2((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2Br

Base Information

• Chemical Name: WBr(CO)2((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2⁽¹⁺⁾*Br^(1-)=WBr(CO)2((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2Br
• CAS No.: 80010-26-0
• Molecular Formula: Br*C₅₄H₄₈BrO₂P₄W
• Molecular Weight: 1196.53
• Mol file: 80010-26-0.mol

Synonyms:WBr(CO)2((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2⁽¹⁺⁾*Br^(1-)=WBr(CO)2((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2Br

Chemical Property of WBr(CO)2((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2⁽¹⁺⁾*Br^(1-)=WBr(CO)2((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2Br

Chemical Property:

Purity/Quality:

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Technology Process of WBr(CO)2((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2⁽¹⁺⁾*Br^(1-)=WBr(CO)2((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2Br

There total 1 articles about WBr(CO)2((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2⁽¹⁺⁾*Br^(1-)=WBr(CO)2((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2Br which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

dibromotricarbonyl(N-(p-tolyltriphenylphosphoranyliden)triazene)tungsten(II) (80594-73-6) → WBr(CO)2((C6H5)2PCH2CH2P(C6H5)2)2(1+)*Br(1-)=WBr(CO)2((C6H5)2PCH2CH2P(C6H5)2)2Br (80010-26-0)

Guidance literature:

With P(C₆H₅)2CH₂CH₂P(C₆H₅)2; In dichloromethane; diphos addind to W complex in CH2Cl2 under N2, stirring for 1 h at ambient temp., solvent removing in vacuo, toluene adding, refluxing for 1 h,yellow ppt. filtering off and washing with hexane; identified by IR spectrum;

DOI:10.1021/ic00135a068

upstream raw materials:

dibromotricarbonyl(N-(p-tolyltriphenylphosphoranyliden)triazene)tungsten(II)