3-Methyl-5-phenyl-isotellurazole

Base Information

• Chemical Name: 3-Methyl-5-phenyl-isotellurazole
• CAS No.: 88459-86-3
• Molecular Formula: C₁₀H₉NTe
• Molecular Weight: 270.788
• Mol file: 88459-86-3.mol

Synonyms:3-Methyl-5-phenyl-isotellurazole

Chemical Property of 3-Methyl-5-phenyl-isotellurazole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-Methyl-5-phenyl-isotellurazole

There total 8 articles about 3-Methyl-5-phenyl-isotellurazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

C10H9NOTe (936924-43-5) → 3-Methyl-5-phenyl-isotellurazole (88459-86-3)

Guidance literature:

With triphenylphosphine; In chloroform; at 100 ℃; for 12h;

DOI:10.1246/bcsj.80.567

Reference yield: 79.0%

dimethyl-tellurocarbamic acid Te-(3-oxo-1-phenyl-but-1-enyl) ester (858641-30-2) → C10H9NOTe (936924-43-5) + 3-Methyl-5-phenyl-isotellurazole (88459-86-3)

Guidance literature:

With hydroxylamine-O-sulfonic acid; In methanol; for 2h; Heating;

DOI:10.1246/bcsj.80.567

Reference yield: 30.0%

bis(N,N-dimethylcarbamoyl) ditelluride (106011-93-2) + C17H15NO3S (255390-22-8) → C20H22N2O4STe + 3-Methyl-5-phenyl-isotellurazole (88459-86-3)

Guidance literature:

bis(N,N-dimethylcarbamoyl) ditelluride; With sodium tetrahydroborate; In methanol; at -50 ℃; for 0.25h;

C₁₇H₁₅NO₃S; In methanol; at 40 ℃; for 7h; Further stages.;

DOI:10.1246/bcsj.80.567

upstream raw materials:

dimethyl-tellurocarbamic acid Te-(3-oxo-1-phenyl-but-1-enyl) ester

C₁₀H₉NOTe

bis(N,N-dimethylcarbamoyl) ditelluride

C₁₇H₁₅NO₃S

Downstream raw materials:

C₁₉H₁₅NO

C₁₈H₂₁NO₂

C₁₅H₁₆N₂O

C₁₇H₂₁NOSi