C₁₈H₁₆⁽²⁾H₃BrO

Base Information

Chemical Name:C₁₈H₁₆⁽²⁾H₃BrO
CAS No.:95249-76-6
Molecular Formula:C₁₈H₁₉BrO
Molecular Weight:334.228
Hs Code.:

C<sub>18</sub>H<sub>16</sub><sup>(2)</sup>H<sub>3</sub>BrO

Synonyms:C₁₈H₁₆⁽²⁾H₃BrO

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈H₁₆⁽²⁾H₃BrO

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Technology Process of C₁₈H₁₆⁽²⁾H₃BrO

There total 7 articles about C₁₈H₁₆⁽²⁾H₃BrO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₄H₂₂⁽²⁾H₃BrOS

: C₁₈H₁₆⁽²⁾H₃BrO

: 95249-76-6
C₁₈H₁₆⁽²⁾H₃BrO

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -70 ℃; for 0.5h; Yield given. Yields of byproduct given;
DOI:10.1021/ja00293a039

Reference yield:

: 36276-24-1
3-bromo-4-methyl-benzaldehyde

: 95249-76-6
C₁₈H₁₆⁽²⁾H₃BrO

Guidance literature:: Multi-step reaction with 4 steps

1: Mg / 1.) Et₂O, 2.) reflux, 0.5 h

2: 50.9 g / formic acid / 26 h

3: 78 percent / 1.) NaNH₂ / diethyl ether; liquid ammonia / 1.) from -45 degC to 0 degC over 3 h; 2., room t, 3 h

4: m-chloroperbenzoic acid / CH₂Cl₂ / 0.5 h / -70 °C

With formic acid; sodium amide; magnesium; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane; ammonia;
DOI:10.1021/ja00293a039

Reference yield:

: 42006-91-7
4-bromobenzyl-α,α-d₂ alcohol

: 95249-76-6
C₁₈H₁₆⁽²⁾H₃BrO

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) SOCl₂, pyridine; 2.) LiEt₃BD / 1.) benzene, reflux, 0.5 h; 2.) THF, room t., 24 h

2: Mg / 1.) Et₂O, 2.) reflux, 0.5 h

3: 50.9 g / formic acid / 26 h

4: 78 percent / 1.) NaNH₂ / diethyl ether; liquid ammonia / 1.) from -45 degC to 0 degC over 3 h; 2., room t, 3 h

5: m-chloroperbenzoic acid / CH₂Cl₂ / 0.5 h / -70 °C

With pyridine; lithium triethyl borodeuteride; formic acid; thionyl chloride; sodium amide; magnesium; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane; ammonia;
DOI:10.1021/ja00293a039