methyl 3-methyl-2-[(3S,4R)-3-[1-methyl-1-(4-nitrobenzyloxycarbonyloxy)ethyl]-4-[2-(4-nitrobenzyloxycarbonyl-methyl)allyl]-2-oxoazetidin-1-yl]but-2-enoate

Base Information

• Chemical Name: methyl 3-methyl-2-[(3S,4R)-3-[1-methyl-1-(4-nitrobenzyloxycarbonyloxy)ethyl]-4-[2-(4-nitrobenzyloxycarbonyl-methyl)allyl]-2-oxoazetidin-1-yl]but-2-enoate
• CAS No.: 86489-10-3
• Molecular Formula: C₃₂H₃₅N₃O₁₂
• Molecular Weight: 653.643

Synonyms:methyl 3-methyl-2-[(3S,4R)-3-[1-methyl-1-(4-nitrobenzyloxycarbonyloxy)ethyl]-4-[2-(4-nitrobenzyloxycarbonyl-methyl)allyl]-2-oxoazetidin-1-yl]but-2-enoate

Chemical Property of methyl 3-methyl-2-[(3S,4R)-3-[1-methyl-1-(4-nitrobenzyloxycarbonyloxy)ethyl]-4-[2-(4-nitrobenzyloxycarbonyl-methyl)allyl]-2-oxoazetidin-1-yl]but-2-enoate

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Technology Process of methyl 3-methyl-2-[(3S,4R)-3-[1-methyl-1-(4-nitrobenzyloxycarbonyloxy)ethyl]-4-[2-(4-nitrobenzyloxycarbonyl-methyl)allyl]-2-oxoazetidin-1-yl]but-2-enoate

There total 2 articles about methyl 3-methyl-2-[(3S,4R)-3-[1-methyl-1-(4-nitrobenzyloxycarbonyloxy)ethyl]-4-[2-(4-nitrobenzyloxycarbonyl-methyl)allyl]-2-oxoazetidin-1-yl]but-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 2-[(3S,4R)-4-chloro-3-[1-methyl-1-(4-nitrobenzyloxycarbonyloxy)ethyl]-2-oxoazetidin-1-yl]-3-methylbut-2-enoate (86489-04-5) + p-nitrobenzyl 3-(trimethylsilylmethyl)but-3-enolate (80528-32-1) → methyl 3-methyl-2-[(3S,4R)-3-[1-methyl-1-(4-nitrobenzyloxycarbonyloxy)ethyl]-4-[2-(4-nitrobenzyloxycarbonyl-methyl)allyl]-2-oxoazetidin-1-yl]but-2-enoate (86489-10-3)

Guidance literature:

With silver tetrafluoroborate; sodium chloride; sodium hydrogencarbonate; In dichloromethane; acetone;

Reference yield:

methyl 2-[(3S,4R)-4-chloro-3-[1-methyl-1-(4-nitrobenzyloxycarbonyloxy)ethyl]-2-oxoazetidin-1-yl]-3-methylbut-2-enoate (86489-04-5) → methyl 3-methyl-2-[(3S,4R)-3-[1-methyl-1-(4-nitrobenzyloxycarbonyloxy)ethyl]-4-[2-(4-nitrobenzyloxycarbonyl-methyl)allyl]-2-oxoazetidin-1-yl]but-2-enoate (86489-10-3)

Guidance literature:

Reference yield:

methyl 3-methyl-2-[(3S,4R)-3-[1-methyl-1-(4-nitrobenzyloxycarbonyloxy)ethyl]-4-[2-(4-nitrobenzyloxycarbonyl-methyl)allyl]-2-oxoazetidin-1-yl]but-2-enoate (86489-10-3) → 4-nitrobenzyl 4-[(2R,3S)-3-[1-methyl-1-(4-nitrobenzyloxycarbonyloxy)ethyl]-4-oxoazetidin-2-yl]-3-oxobutanoate (86489-43-2)

Guidance literature:

With dimethylsulfide; sodium hydrogensulfite; In methanol; dichloromethane; ethyl acetate; acetone;

upstream raw materials:

methyl 2-[(3S,4R)-4-chloro-3-[1-methyl-1-(4-nitrobenzyloxycarbonyloxy)ethyl]-2-oxoazetidin-1-yl]-3-methylbut-2-enoate

p-nitrobenzyl 3-(trimethylsilylmethyl)but-3-enolate

Downstream raw materials:

4-nitrobenzyl 4-[(2R,3S)-3-[1-methyl-1-(4-nitrobenzyloxycarbonyloxy)ethyl]-4-oxoazetidin-2-yl]-3-oxobutanoate

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