1-(Prop-2-en-1-yl)cyclohex-3-ene-1-carbonyl chloride

Base Information

Chemical Name:1-(Prop-2-en-1-yl)cyclohex-3-ene-1-carbonyl chloride
CAS No.:76403-28-6
Molecular Formula:C₁₀H₁₃ClO
Molecular Weight:184.666
Hs Code.:
DSSTox Substance ID:DTXSID90505731
Mol file:76403-28-6.mol

Synonyms:76403-28-6;1-(Prop-2-en-1-yl)cyclohex-3-ene-1-carbonyl chloride;DTXSID90505731

Suppliers and Price of 1-(Prop-2-en-1-yl)cyclohex-3-ene-1-carbonyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1-(Prop-2-en-1-yl)cyclohex-3-ene-1-carbonyl chloride

Chemical Property:

PSA：17.07000
LogP:3.05440
XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:184.0654927
Heavy Atom Count:12
Complexity:220

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CCC1(CCC=CC1)C(=O)Cl

Technology Process of 1-(Prop-2-en-1-yl)cyclohex-3-ene-1-carbonyl chloride

There total 2 articles about 1-(Prop-2-en-1-yl)cyclohex-3-ene-1-carbonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76403-27-5
1-Allyl-cyclohex-3-enecarboxylic acid

: 76403-28-6
1-Allyl-cyclohex-3-enecarbonyl chloride

Guidance literature:: With thionyl chloride; at 25 ℃; for 1h;
DOI:10.1021/jo00321a017

Reference yield:

: 4771-80-6
1,2,5,6-tetrahydrobenzoic acid

: 76403-28-6
1-Allyl-cyclohex-3-enecarbonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: lithium diisopropylamide / 1.) THF, 0 deg C, then 25 deg C, 1 h and 60 deg C, 0.5 h, 2.) 0 deg C, then 25 deg C, 16 h

2: thionyl chloride / 1 h / 25 °C

With thionyl chloride; lithium diisopropyl amide;
DOI:10.1021/jo00321a017