5-[3-(5-{3-[5-(3-bromo-phenyl)-[1,3,4]oxadiazol-2-yl]-phenyl}-[1,3,4]oxadiazol-2-yl)-phenyl]-1⁽²⁾H-tetrazole

Base Information

• Chemical Name: 5-[3-(5-{3-[5-(3-bromo-phenyl)-[1,3,4]oxadiazol-2-yl]-phenyl}-[1,3,4]oxadiazol-2-yl)-phenyl]-1⁽²⁾H-tetrazole
• CAS No.: 47750-18-5
• Molecular Formula: C₂₃H₁₃BrN₈O₂
• Molecular Weight: 513.313

Synonyms:5-[3-(5-{3-[5-(3-bromo-phenyl)-[1,3,4]oxadiazol-2-yl]-phenyl}-[1,3,4]oxadiazol-2-yl)-phenyl]-1⁽²⁾H-tetrazole

Chemical Property of 5-[3-(5-{3-[5-(3-bromo-phenyl)-[1,3,4]oxadiazol-2-yl]-phenyl}-[1,3,4]oxadiazol-2-yl)-phenyl]-1⁽²⁾H-tetrazole

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Technology Process of 5-[3-(5-{3-[5-(3-bromo-phenyl)-[1,3,4]oxadiazol-2-yl]-phenyl}-[1,3,4]oxadiazol-2-yl)-phenyl]-1⁽²⁾H-tetrazole

There total 4 articles about 5-[3-(5-{3-[5-(3-bromo-phenyl)-[1,3,4]oxadiazol-2-yl]-phenyl}-[1,3,4]oxadiazol-2-yl)-phenyl]-1⁽²⁾H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-(3-bromophenyl)-2H-tetrazole (3440-99-1) → 5-[3-(5-{3-[5-(3-bromo-phenyl)-[1,3,4]oxadiazol-2-yl]-phenyl}-[1,3,4]oxadiazol-2-yl)-phenyl]-1(2)H-tetrazole (47750-18-5)

Guidance literature:

Multi-step reaction with 4 steps

1: Py / 100 °C

2: LiCl, NaN₃ / 2-methoxy-ethanol / Heating

3: Py / Heating

4: LiN₃ / 2-methoxy-ethanol / Heating

With pyridine; sodium azide; lithium azide; lithium chloride; In 2-methoxy-ethanol;

Reference yield:

3-[5-(3-bromo-phenyl)-[1,3,4]oxadiazol-2-yl]-benzonitrile (3477-83-6) → 5-[3-(5-{3-[5-(3-bromo-phenyl)-[1,3,4]oxadiazol-2-yl]-phenyl}-[1,3,4]oxadiazol-2-yl)-phenyl]-1(2)H-tetrazole (47750-18-5)

Guidance literature:

Multi-step reaction with 3 steps

1: LiCl, NaN₃ / 2-methoxy-ethanol / Heating

2: Py / Heating

3: LiN₃ / 2-methoxy-ethanol / Heating

With pyridine; sodium azide; lithium azide; lithium chloride; In 2-methoxy-ethanol;

Reference yield:

3-cyanobenzoyl chloride (1711-11-1) → 5-[3-(5-{3-[5-(3-bromo-phenyl)-[1,3,4]oxadiazol-2-yl]-phenyl}-[1,3,4]oxadiazol-2-yl)-phenyl]-1(2)H-tetrazole (47750-18-5)

Guidance literature:

Multi-step reaction with 4 steps

1: Py / 100 °C

2: LiCl, NaN₃ / 2-methoxy-ethanol / Heating

3: Py / Heating

4: LiN₃ / 2-methoxy-ethanol / Heating

With pyridine; sodium azide; lithium azide; lithium chloride; In 2-methoxy-ethanol;

upstream raw materials:

5-(3-bromophenyl)-2H-tetrazole

3-[5-(3-bromo-phenyl)-[1,3,4]oxadiazol-2-yl]-benzonitrile

3-cyanobenzoyl chloride

5-{3-[5-(3-bromo-phenyl)-[1,3,4]oxadiazol-2-yl]-phenyl}-1⁽²⁾H-tetrazole

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