C₂₄H₁₉NO₅

Base Information

• Chemical Name: C₂₄H₁₉NO₅
• CAS No.: 1307863-96-2
• Molecular Formula: C₂₄H₁₉NO₅
• Molecular Weight: 401.419
• Mol file: 1307863-96-2.mol

Synonyms:C₂₄H₁₉NO₅

Chemical Property of C₂₄H₁₉NO₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₁₉NO₅

There total 8 articles about C₂₄H₁₉NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

C25H21NO5 (1373514-02-3) → C24H19NO5 (1307863-96-2)

Guidance literature:

C₂₅H₂₁NO₅; With boron tribromide; In dichloromethane; at 20 ℃; for 4h;

With methanol; In dichloromethane; at 0 - 20 ℃; for 16h;

DOI:10.1039/c2ob00022a

Reference yield:

1-bromo-4-methoxy-benzene (104-92-7) → C24H19NO5 (1307863-96-2)

Guidance literature:

Multi-step reaction with 4 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere

1.2: 145 °C / Inert atmosphere

2.1: potassium hydroxide / water / 4 h / Inert atmosphere; Reflux

3.1: pyridine; p-toluenesulfonyl chloride / 4 h / 20 °C / Inert atmosphere

4.1: boron tribromide / dichloromethane / 4 h / 20 °C

4.2: 16 h / 0 - 20 °C

With pyridine; boron tribromide; sodium hydride; p-toluenesulfonyl chloride; potassium hydroxide; In dichloromethane; water; N,N-dimethyl-formamide; mineral oil;

DOI:10.1039/c2ob00022a

Reference yield:

2-methoxyacridine-9-carboxylic acid (130266-57-8) → C24H19NO5 (1307863-96-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: pyridine; p-toluenesulfonyl chloride / 4 h / 20 °C / Inert atmosphere

2.1: boron tribromide / dichloromethane / 4 h / 20 °C

2.2: 16 h / 0 - 20 °C

With pyridine; boron tribromide; p-toluenesulfonyl chloride; In dichloromethane;

DOI:10.1039/c2ob00022a

upstream raw materials:

1-bromo-4-methoxy-benzene

2-methoxyacridine-9-carboxylic acid

C₉H₉ClO₂

C₂₅H₂₁NO₅

Downstream raw materials:

C₃₂H₃₆N₂O₅

C₂₉H₃₀N₂O₅

C₃₀H₃₁NO₈S

C₃₉H₄₉NO₁₄S