tert-butyl 4-(((1-(3,4,5-trimethoxybenzyl)-1H-1,2,3-triazol-4-yl)methylthio)carbonothioyl)piperazine-1-carboxylate

Base Information

• Chemical Name: tert-butyl 4-(((1-(3,4,5-trimethoxybenzyl)-1H-1,2,3-triazol-4-yl)methylthio)carbonothioyl)piperazine-1-carboxylate
• CAS No.: 1418150-20-5
• Molecular Formula: C₂₃H₃₃N₅O₅S₂
• Molecular Weight: 523.678

Synonyms:tert-butyl 4-(((1-(3,4,5-trimethoxybenzyl)-1H-1,2,3-triazol-4-yl)methylthio)carbonothioyl)piperazine-1-carboxylate

Chemical Property of tert-butyl 4-(((1-(3,4,5-trimethoxybenzyl)-1H-1,2,3-triazol-4-yl)methylthio)carbonothioyl)piperazine-1-carboxylate

Chemical Property:

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Technology Process of tert-butyl 4-(((1-(3,4,5-trimethoxybenzyl)-1H-1,2,3-triazol-4-yl)methylthio)carbonothioyl)piperazine-1-carboxylate

There total 2 articles about tert-butyl 4-(((1-(3,4,5-trimethoxybenzyl)-1H-1,2,3-triazol-4-yl)methylthio)carbonothioyl)piperazine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-t-Butoxycarbonylpiperazine (57260-71-6) → tert-butyl 4-(((1-(3,4,5-trimethoxybenzyl)-1H-1,2,3-triazol-4-yl)methylthio)carbonothioyl)piperazine-1-carboxylate (1418150-20-5)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium phosphate dodecahydrate / acetone / 0.5 h / 20 °C

2: acetone / 0.5 h / 20 °C

3: copper(ll) sulfate pentahydrate; sodium L-ascorbate / tetrahydrofuran; water / 20 °C

With sodium phosphate dodecahydrate; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In tetrahydrofuran; water; acetone;

DOI:10.1016/j.ejmech.2012.12.046

Reference yield:

C10H18N2O2S2 (773024-43-4) → tert-butyl 4-(((1-(3,4,5-trimethoxybenzyl)-1H-1,2,3-triazol-4-yl)methylthio)carbonothioyl)piperazine-1-carboxylate (1418150-20-5)

Guidance literature:

Multi-step reaction with 2 steps

1: acetone / 0.5 h / 20 °C

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / tetrahydrofuran; water / 20 °C

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In tetrahydrofuran; water; acetone;

DOI:10.1016/j.ejmech.2012.12.046

Reference yield:

tert-butyl 4-(((1-(3,4,5-trimethoxybenzyl)-1H-1,2,3-triazol-4-yl)methylthio)carbonothioyl)piperazine-1-carboxylate (1418150-20-5) → (1-(3,4,5-trimethoxybenzyl)-1H-1,2,3-triazol-4-yl)methyl piperazine-1-carbodithioate (1418150-35-2)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃;

DOI:10.1016/j.ejmech.2012.12.046

upstream raw materials:

C₁₀H₁₈N₂O₂S₂

1-t-Butoxycarbonylpiperazine

Downstream raw materials:

(1-(3,4,5-trimethoxybenzyl)-1H-1,2,3-triazol-4-yl)methyl piperazine-1-carbodithioate

benzyl 4-(((1-(3,4,5-trimethoxybenzyl)-1H-1,2,3-triazol-4-yl)methylthio)carbonthioyl)piperazine-1-carboxylate

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