cyclopropanecarboxylic acid 4-(1-cyclopropanecarbonyl-piperidin-4-ylmethyl)-3-oxo-2-(2,4,6-trimethyl-phenyl)-cyclopent-1-enyl ester

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Chemical Name:cyclopropanecarboxylic acid 4-(1-cyclopropanecarbonyl-piperidin-4-ylmethyl)-3-oxo-2-(2,4,6-trimethyl-phenyl)-cyclopent-1-enyl ester
CAS No.:1203554-99-7
Molecular Formula:C₂₈H₃₅NO₄
Molecular Weight:449.59
Hs Code.:

Synonyms:cyclopropanecarboxylic acid 4-(1-cyclopropanecarbonyl-piperidin-4-ylmethyl)-3-oxo-2-(2,4,6-trimethyl-phenyl)-cyclopent-1-enyl ester

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Chemical Property of cyclopropanecarboxylic acid 4-(1-cyclopropanecarbonyl-piperidin-4-ylmethyl)-3-oxo-2-(2,4,6-trimethyl-phenyl)-cyclopent-1-enyl ester

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Technology Process of cyclopropanecarboxylic acid 4-(1-cyclopropanecarbonyl-piperidin-4-ylmethyl)-3-oxo-2-(2,4,6-trimethyl-phenyl)-cyclopent-1-enyl ester

There total 7 articles about cyclopropanecarboxylic acid 4-(1-cyclopropanecarbonyl-piperidin-4-ylmethyl)-3-oxo-2-(2,4,6-trimethyl-phenyl)-cyclopent-1-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1203552-90-2
4-[2,4-dioxo-3-(2,4,6-trimethyl-phenyl)-cyclopentylmethyl]-piperidinium hydrochloride

: 4023-34-1
cyclopropanecarboxylic acid chloride

: 1203554-99-7
cyclopropanecarboxylic acid 4-(1-cyclopropanecarbonyl-piperidin-4-ylmethyl)-3-oxo-2-(2,4,6-trimethyl-phenyl)-cyclopent-1-enyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 5h;

Reference yield:

: 4-[2,4-dioxo-3-(2,4,6-trimethyl-phenyl)cyclopentylmethyl]piperidinium hydrochloride

: 4023-34-1
cyclopropanecarboxylic acid chloride

: 1203554-99-7
cyclopropanecarboxylic acid 4-(1-cyclopropanecarbonyl-piperidin-4-ylmethyl)-3-oxo-2-(2,4,6-trimethyl-phenyl)-cyclopent-1-enyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 5h;

Reference yield:

: 84629-38-9
3-methoxy-2-(2,4,6-trimethylphenyl)-cyclopent-2-en-1-one

: 1203554-99-7
cyclopropanecarboxylic acid 4-(1-cyclopropanecarbonyl-piperidin-4-ylmethyl)-3-oxo-2-(2,4,6-trimethyl-phenyl)-cyclopent-1-enyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium hexamethyldisilazane / hexane; tetrahydrofuran; ethylbenzene / 1 h / -78 °C / Inert atmosphere

1.2: 1.5 h / -78 - 20 °C

1.3: 2 h / 20 °C

2.1: hydrogen / palladium 10% on activated carbon / ethanol / 3000.3 Torr

3.1: hydrogenchloride; water / acetone / 4 h / Reflux

4.1: triethylamine / dichloromethane / 5 h / 20 °C

With hydrogenchloride; water; hydrogen; triethylamine; lithium hexamethyldisilazane; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; hexane; dichloromethane; ethylbenzene; acetone;