C₅₅H₆₀N₂S₃Si₂

Base Information

Chemical Name:C₅₅H₆₀N₂S₃Si₂
CAS No.:1352135-56-8
Molecular Formula:C₅₅H₆₀N₂S₃Si₂
Molecular Weight:901.464
Hs Code.:

C<sub>55</sub>H<sub>60</sub>N<sub>2</sub>S<sub>3</sub>Si<sub>2</sub>

Synonyms:C₅₅H₆₀N₂S₃Si₂

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Chemical Property of C₅₅H₆₀N₂S₃Si₂

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Technology Process of C₅₅H₆₀N₂S₃Si₂

There total 5 articles about C₅₅H₆₀N₂S₃Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1352135-53-5
C₄₅H₄₂Br₂N₂S₃

: 1066-54-2
trimethylsilylacetylene

: 1352135-56-8
C₅₅H₆₀N₂S₃Si₂

Guidance literature:: C₄₅H₄₂Br₂N₂S₃; With copper(l) iodide; palladium diacetate; triethylamine; triphenylphosphine; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;

trimethylsilylacetylene; In dichloromethane; at 0 ℃; Inert atmosphere; Reflux;
DOI:10.1016/j.jorganchem.2011.07.005

Reference yield:

: 498-62-4
3-thiophene carboxaldehyde

: 1352135-56-8
C₅₅H₆₀N₂S₃Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogen bromide; bromine / diethyl ether

2.1: ammonium acetate / acetic acid / 123 °C / Inert atmosphere

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 24 h / Inert atmosphere; Reflux

4.1: N-Bromosuccinimide / tetrahydrofuran / 20 °C / Inert atmosphere; Darkness

5.1: copper(l) iodide; palladium diacetate; triethylamine; triphenylphosphine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

5.2: 0 °C / Inert atmosphere; Reflux

With N-Bromosuccinimide; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonium acetate; hydrogen bromide; bromine; palladium diacetate; triethylamine; triphenylphosphine; In tetrahydrofuran; diethyl ether; dichloromethane; acetic acid; toluene; 3.1: Stille cross-coupling / 5.1: Sonogashira coupling reaction / 5.2: Sonogashira coupling reaction;
DOI:10.1016/j.jorganchem.2011.07.005

Reference yield:

: 1001425-37-1
2-(2,5-dibromothiophen-3-yl)-1-phenyl-1H-phenanthro[9,10-d]imidazole

: 1352135-56-8
C₅₅H₆₀N₂S₃Si₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 24 h / Inert atmosphere; Reflux

2.1: N-Bromosuccinimide / tetrahydrofuran / 20 °C / Inert atmosphere; Darkness

3.1: copper(l) iodide; palladium diacetate; triethylamine; triphenylphosphine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

3.2: 0 °C / Inert atmosphere; Reflux

With N-Bromosuccinimide; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium diacetate; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; toluene; 1.1: Stille cross-coupling / 3.1: Sonogashira coupling reaction / 3.2: Sonogashira coupling reaction;
DOI:10.1016/j.jorganchem.2011.07.005