C₁₆H₁₇BrFN₃O₄S

Base Information

Chemical Name:C₁₆H₁₇BrFN₃O₄S
CAS No.:1312435-90-7
Molecular Formula:C₁₆H₁₇BrFN₃O₄S
Molecular Weight:446.297
Hs Code.:

C<sub>16</sub>H<sub>17</sub>BrFN<sub>3</sub>O<sub>4</sub>S

Synonyms:C₁₆H₁₇BrFN₃O₄S

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Chemical Property of C₁₆H₁₇BrFN₃O₄S

Chemical Property:

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Technology Process of C₁₆H₁₇BrFN₃O₄S

There total 1 articles about C₁₆H₁₇BrFN₃O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 40052-13-9
mono-tert-butyl malonate

: 1312435-89-4
C₉H₇BrFN₃OS

: 1312435-90-7
C₁₆H₁₇BrFN₃O₄S

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 3h; Inert atmosphere;

Reference yield:

: 1312435-90-7
C₁₆H₁₇BrFN₃O₄S

: 1312435-92-9
C₂₂H₂₀FN₃O₃S

Guidance literature:: Multi-step reaction with 2 steps

1: Burgess Reagent / 1,4-dioxane / 2 h / 90 °C

2: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 0.5 h / 120 °C / Inert atmosphere; Microwave irradiation

With Burgess Reagent; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; water;

Reference yield:

: 1312435-90-7
C₁₆H₁₇BrFN₃O₄S

: 1312435-93-0
C₁₈H₁₂FN₃O₃S

Guidance literature:: Multi-step reaction with 3 steps

1: Burgess Reagent / 1,4-dioxane / 2 h / 90 °C

2: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 0.5 h / 120 °C / Inert atmosphere; Microwave irradiation

3: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

With Burgess Reagent; sodium carbonate; trifluoroacetic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; dichloromethane; water;