(S,E)-1-(5-methoxy-2-nitro-4-(4-(4-(4-oxo-2-styrylquinazolin-3(4H)-yl)phenoxy)butoxy)benzoyl)pyrrolidine-2-carbaldehyde diethyl dithioacetal

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Chemical Name:(S,E)-1-(5-methoxy-2-nitro-4-(4-(4-(4-oxo-2-styrylquinazolin-3(4H)-yl)phenoxy)butoxy)benzoyl)pyrrolidine-2-carbaldehyde diethyl dithioacetal
CAS No.:1214739-97-5
Molecular Formula:C₄₃H₄₆N₄O₇S₂
Molecular Weight:794.993
Hs Code.:

Synonyms:(S,E)-1-(5-methoxy-2-nitro-4-(4-(4-(4-oxo-2-styrylquinazolin-3(4H)-yl)phenoxy)butoxy)benzoyl)pyrrolidine-2-carbaldehyde diethyl dithioacetal

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Chemical Property of (S,E)-1-(5-methoxy-2-nitro-4-(4-(4-(4-oxo-2-styrylquinazolin-3(4H)-yl)phenoxy)butoxy)benzoyl)pyrrolidine-2-carbaldehyde diethyl dithioacetal

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Technology Process of (S,E)-1-(5-methoxy-2-nitro-4-(4-(4-(4-oxo-2-styrylquinazolin-3(4H)-yl)phenoxy)butoxy)benzoyl)pyrrolidine-2-carbaldehyde diethyl dithioacetal

There total 2 articles about (S,E)-1-(5-methoxy-2-nitro-4-(4-(4-(4-oxo-2-styrylquinazolin-3(4H)-yl)phenoxy)butoxy)benzoyl)pyrrolidine-2-carbaldehyde diethyl dithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1214739-97-5
(S,E)-1-(5-methoxy-2-nitro-4-(4-(4-(4-oxo-2-styrylquinazolin-3(4H)-yl)phenoxy)butoxy)benzoyl)pyrrolidine-2-carbaldehyde diethyl dithioacetal

Guidance literature:

Reference yield: 80.0%

: 1214739-79-3
(E)-3-(4-(4-bromobutoxy)phenyl)-2-styrylquinazolin-4(3H)-one

: 140647-02-5
(2S)-N-(4-hydroxy-5-methoxy-2-nitrobenzoyl)pyrrolidine-2-carboxaldehyde diethyl thioacetal

: 1214739-97-5
(S,E)-1-(5-methoxy-2-nitro-4-(4-(4-(4-oxo-2-styrylquinazolin-3(4H)-yl)phenoxy)butoxy)benzoyl)pyrrolidine-2-carbaldehyde diethyl dithioacetal

Guidance literature:: With potassium carbonate; In acetone; Reflux;
DOI:10.1016/j.bmc.2009.12.015

Reference yield:

: 1214739-97-5
(S,E)-1-(5-methoxy-2-nitro-4-(4-(4-(4-oxo-2-styrylquinazolin-3(4H)-yl)phenoxy)butoxy)benzoyl)pyrrolidine-2-carbaldehyde diethyl dithioacetal

: 1227667-13-1
C₄₃H₄₈N₄O₅S₂

Guidance literature:: (S,E)-1-(5-methoxy-2-nitro-4-(4-(4-(4-oxo-2-styrylquinazolin-3(4H)-yl)phenoxy)butoxy)benzoyl)pyrrolidine-2-carbaldehyde diethyl dithioacetal; With tin(II) chloride dihdyrate; In methanol; Reflux;

With sodium hydrogencarbonate; In water; pH=8;
DOI:10.1016/j.bmc.2009.12.015