1-Phenyl-9H-pyrido[3,4-b]indole-5,6-diamine

Base Information

Chemical Name:1-Phenyl-9H-pyrido[3,4-b]indole-5,6-diamine
CAS No.:131203-82-2
Molecular Formula:C₁₇H₁₄N₄
Molecular Weight:274.325
Hs Code.:
DSSTox Substance ID:DTXSID801262756

Synonyms:1-Phenyl-9H-pyrido[3,4-b]indole-5,6-diamine;DTXSID801262756;131203-82-2

Suppliers and Price of 1-Phenyl-9H-pyrido[3,4-b]indole-5,6-diamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Phenyl-9H-pyrido[3,4-b]indole-5,6-diamine

Chemical Property:

XLogP3:2.6
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:274.121846464
Heavy Atom Count:21
Complexity:368

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=NC=CC3=C2NC4=C3C(=C(C=C4)N)N

Technology Process of 1-Phenyl-9H-pyrido[3,4-b]indole-5,6-diamine

There total 4 articles about 1-Phenyl-9H-pyrido[3,4-b]indole-5,6-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 131203-80-0
5-Nitro-1-phenyl-9H-β-carbolin-6-ylamine

: 131203-82-2
5,6-diamino-1-phenyl-9H-pyrido<3,4-b>indole

Guidance literature:: With hydrogen; nickel; In ethanol; for 6h; under 2206.5 Torr;

Reference yield:

: 127042-69-7
6-amino-1-phenyl-9H-pyrido<3,4-b>indole

: 131203-82-2
5,6-diamino-1-phenyl-9H-pyrido<3,4-b>indole

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / 0.5 h / 100 °C

2: 72 percent / conc. HNO₃ / 0.5 h

3: 99 percent / 10percent aq. NaOH / ethanol / 0.5 h / Heating

4: 99 percent / H₂ / Raney nickel / ethanol / 6 h / 2206.5 Torr

With sodium hydroxide; hydrogen; nitric acid; nickel; In ethanol;

Reference yield:

: 131219-84-6
N-(1-Phenyl-9H-β-carbolin-6-yl)-acetamide

: 131203-82-2
5,6-diamino-1-phenyl-9H-pyrido<3,4-b>indole

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / conc. HNO₃ / 0.5 h

2: 99 percent / 10percent aq. NaOH / ethanol / 0.5 h / Heating

3: 99 percent / H₂ / Raney nickel / ethanol / 6 h / 2206.5 Torr

With sodium hydroxide; hydrogen; nitric acid; nickel; In ethanol;