1-({[(2E)-4,4-dimethoxy-3-methylbut-2-en-1-yl]oxy}methyl)-4-methoxybenzene

Base Information

Chemical Name:1-({[(2E)-4,4-dimethoxy-3-methylbut-2-en-1-yl]oxy}methyl)-4-methoxybenzene
CAS No.:329188-96-7
Molecular Formula:C₁₅H₂₂O₄
Molecular Weight:266.337
Hs Code.:

Synonyms:1-({[(2E)-4,4-dimethoxy-3-methylbut-2-en-1-yl]oxy}methyl)-4-methoxybenzene

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Chemical Property of 1-({[(2E)-4,4-dimethoxy-3-methylbut-2-en-1-yl]oxy}methyl)-4-methoxybenzene

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Technology Process of 1-({[(2E)-4,4-dimethoxy-3-methylbut-2-en-1-yl]oxy}methyl)-4-methoxybenzene

There total 4 articles about 1-({[(2E)-4,4-dimethoxy-3-methylbut-2-en-1-yl]oxy}methyl)-4-methoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53892-77-6
(E/Z)-4-Hydroxy-2-methyl-2-butenal-dimethylacetal

: 824-94-2
p-methoxybenzyl chloride

: 1-({[(2Z)-4,4-dimethoxy-3-methylbut-2-en-1-yl]oxy}methyl)-4-methoxybenzene

: 329188-96-7
1-({[(2E)-4,4-dimethoxy-3-methylbut-2-en-1-yl]oxy}methyl)-4-methoxybenzene

Guidance literature:: (E/Z)-4-Hydroxy-2-methyl-2-butenal-dimethylacetal; With sodium hydride; In 1,2-dimethoxyethane; at 0 ℃; for 0.333333h;

p-methoxybenzyl chloride; With sodium iodide; In 1,2-dimethoxyethane; at 20 ℃; for 0.75h;

Reference yield:

: 121289-23-4
p-methoxybenzyloxyacetaldehyde

: 329188-96-7
1-({[(2E)-4,4-dimethoxy-3-methylbut-2-en-1-yl]oxy}methyl)-4-methoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 80 °C

2: NH₄Cl / methanol

With ammonium chloride; In methanol; toluene;
DOI:10.1002/1521-3773(20010105)40:1<231::AID-ANIE231>3.0.CO;2-W

Reference yield:

: 2746-25-0
p-Methoxybenzyl bromide

: 329188-96-7
1-({[(2E)-4,4-dimethoxy-3-methylbut-2-en-1-yl]oxy}methyl)-4-methoxybenzene

Guidance literature:: Multi-step reaction with 4 steps

1.1: 72 percent / NaH / dimethylformamide

2.1: O₃ / CH₂Cl₂ / -78 °C

2.2: Ph₃P / CH₂Cl₂ / 20 °C

3.1: toluene / 80 °C

4.1: NH₄Cl / methanol

With sodium hydride; ammonium chloride; ozone; In methanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1002/1521-3773(20010105)40:1<231::AID-ANIE231>3.0.CO;2-W