(Z,Z)-methyl 2-[1,3-dibenzyl-1,3,4',5'-tetrahydro-4'-methyl-2'-(phenylimino)spiro[2H-benzo[d]imidazole-2,3'(2'H)-thiophen]-5'-ylidene]acetate

Base Information

• Chemical Name: (Z,Z)-methyl 2-[1,3-dibenzyl-1,3,4',5'-tetrahydro-4'-methyl-2'-(phenylimino)spiro[2H-benzo[d]imidazole-2,3'(2'H)-thiophen]-5'-ylidene]acetate
• CAS No.: 1123535-01-2
• Molecular Formula: C₃₄H₃₁N₃O₂S
• Molecular Weight: 545.705

Synonyms:(Z,Z)-methyl 2-[1,3-dibenzyl-1,3,4',5'-tetrahydro-4'-methyl-2'-(phenylimino)spiro[2H-benzo[d]imidazole-2,3'(2'H)-thiophen]-5'-ylidene]acetate

Chemical Property of (Z,Z)-methyl 2-[1,3-dibenzyl-1,3,4',5'-tetrahydro-4'-methyl-2'-(phenylimino)spiro[2H-benzo[d]imidazole-2,3'(2'H)-thiophen]-5'-ylidene]acetate

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Technology Process of (Z,Z)-methyl 2-[1,3-dibenzyl-1,3,4',5'-tetrahydro-4'-methyl-2'-(phenylimino)spiro[2H-benzo[d]imidazole-2,3'(2'H)-thiophen]-5'-ylidene]acetate

There total 2 articles about (Z,Z)-methyl 2-[1,3-dibenzyl-1,3,4',5'-tetrahydro-4'-methyl-2'-(phenylimino)spiro[2H-benzo[d]imidazole-2,3'(2'H)-thiophen]-5'-ylidene]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

methyl 2,3-pentadienoate (22377-44-2) + 1,3-dibenzyl-2-N-phenylthiocarbamoylbenzimidazolium inner salt (211240-97-0) → (Z)-methyl 2-[1,3-dibenzyl-1,3-dihydro-4'-methyl-1'-phenyl-2'-thioxospiro[2H-benzo[d]imidazole-2,3'-pyrrolidine]-5'-ylidene]acetate (1123535-06-7) + (Z,Z)-methyl 2-[1,3-dibenzyl-1,3,4',5'-tetrahydro-4'-methyl-2'-(phenylimino)spiro[2H-benzo[d]imidazole-2,3'(2'H)-thiophen]-5'-ylidene]acetate (1123535-01-2)

Guidance literature:

In benzene; at 80 - 90 ℃; for 2h; regioselective reaction; Inert atmosphere;

DOI:10.1021/jo802687m

Reference yield: 56.0%

methyl 2,3-pentadienoate (22377-44-2) + 1,3-dibenzyl-2-N-phenylthiocarbamoylbenzimidazolium inner salt (211240-97-0) → (Z,Z)-methyl 2-[1,3-dibenzyl-1,3,4',5'-tetrahydro-4'-methyl-2'-(phenylimino)spiro[2H-benzo[d]imidazole-2,3'(2'H)-thiophen]-5'-ylidene]acetate (1123535-01-2)

Guidance literature:

In benzene; at 20 - 30 ℃; for 24h; regioselective reaction; Inert atmosphere;

DOI:10.1021/jo802687m

upstream raw materials:

methyl 2,3-pentadienoate

1,3-dibenzyl-2-N-phenylthiocarbamoylbenzimidazolium inner salt

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