1,1-dimethyl-2-(4-methylphenyl)-4-phenyl-1-silacyclopent-3-ene

Base Information

• Chemical Name: 1,1-dimethyl-2-(4-methylphenyl)-4-phenyl-1-silacyclopent-3-ene
• CAS No.: 1197185-31-1
• Molecular Formula: C₁₉H₂₂Si
• Molecular Weight: 278.469
• Mol file: 1197185-31-1.mol

Synonyms:1,1-dimethyl-2-(4-methylphenyl)-4-phenyl-1-silacyclopent-3-ene

Chemical Property of 1,1-dimethyl-2-(4-methylphenyl)-4-phenyl-1-silacyclopent-3-ene

Chemical Property:

Purity/Quality:

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Technology Process of 1,1-dimethyl-2-(4-methylphenyl)-4-phenyl-1-silacyclopent-3-ene

There total 1 articles about 1,1-dimethyl-2-(4-methylphenyl)-4-phenyl-1-silacyclopent-3-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

2-[(diethylamino)dimethylsilyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane (929887-22-9) + C17H16 (1197185-28-6) → 1,1-dimethyl-2-(4-methylphenyl)-4-phenyl-1-silacyclopent-3-ene (1197185-31-1)

Guidance literature:

With diphenyl(methyl)phosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In toluene; at 20 ℃; for 3h;

DOI:10.1021/ja907170p

Reference yield: 98.0%

1,1-dimethyl-2-(4-methylphenyl)-4-phenyl-1-silacyclopent-3-ene (1197185-31-1) → 1,1-dimethyl-2-(4-methylphenyl)-4-phenylsilole (1197185-35-5)

Guidance literature:

With chloranil; In benzene; at 20 ℃; for 1h; Argon atmosphere;

DOI:10.1021/ja907170p

upstream raw materials:

2-[(diethylamino)dimethylsilyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

C₁₇H₁₆

Downstream raw materials:

1,1-dimethyl-2-(4-methylphenyl)-4-phenylsilole