benzyl 2(R)-2-<<(+)-2-methoxy-2-(trifluoromethyl)-2-phenylacetyl>amino>-3-phenylpropionate

Base Information

Chemical Name:benzyl 2(R)-2-<<(+)-2-methoxy-2-(trifluoromethyl)-2-phenylacetyl>amino>-3-phenylpropionate
CAS No.:126191-15-9
Molecular Formula:C₂₆H₂₄F₃NO₄
Molecular Weight:471.476
Hs Code.:

Synonyms:benzyl 2(R)-2-<<(+)-2-methoxy-2-(trifluoromethyl)-2-phenylacetyl>amino>-3-phenylpropionate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 2(R)-2-<<(+)-2-methoxy-2-(trifluoromethyl)-2-phenylacetyl>amino>-3-phenylpropionate

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Technology Process of benzyl 2(R)-2-<<(+)-2-methoxy-2-(trifluoromethyl)-2-phenylacetyl>amino>-3-phenylpropionate

There total 2 articles about benzyl 2(R)-2-<<(+)-2-methoxy-2-(trifluoromethyl)-2-phenylacetyl>amino>-3-phenylpropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 19803-37-3
Tetrakis(benzyloxy)titanium

: 126253-84-7
(3(2R),4S)-3-<2-<<(+)-2-methoxy-2-(trifluoromethyl)-2-phenylacetyl>amino>-1-oxo-3-phenylpropyl>-4-(phenylmethyl)-2-oxazolidinone

: 126191-15-9
benzyl 2(R)-2-<<(+)-2-methoxy-2-(trifluoromethyl)-2-phenylacetyl>amino>-3-phenylpropionate

Guidance literature:: In benzyl alcohol; at 85 ℃; for 7h;

Reference yield:

: 39637-99-5,20445-33-4
(S)-(+)-2-methoxy-2-trifluoromethyl-2-phenylacetyl chloride

: 126191-15-9
benzyl 2(R)-2-<<(+)-2-methoxy-2-(trifluoromethyl)-2-phenylacetyl>amino>-3-phenylpropionate

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 1 h / 0 °C

2: 89 percent / phenylmethanol / 7 h / 65 - 80 °C

With triethylamine; In dichloromethane; benzyl alcohol;
DOI:10.1016/S0040-4039(00)95305-X