4-{5-[4-(6-acryloyloxy-hexyloxy)-phenyl]-thiophen-2-yl}biphenyl-4-carboxylic acid 6-acryloyloxy-hexyl ester

Base Information

• Chemical Name: 4-{5-[4-(6-acryloyloxy-hexyloxy)-phenyl]-thiophen-2-yl}biphenyl-4-carboxylic acid 6-acryloyloxy-hexyl ester
• CAS No.: 666861-41-2
• Molecular Formula: C₄₁H₄₄O₇S
• Molecular Weight: 680.862
• Mol file: 666861-41-2.mol

Synonyms:4-{5-[4-(6-acryloyloxy-hexyloxy)-phenyl]-thiophen-2-yl}biphenyl-4-carboxylic acid 6-acryloyloxy-hexyl ester

Chemical Property of 4-{5-[4-(6-acryloyloxy-hexyloxy)-phenyl]-thiophen-2-yl}biphenyl-4-carboxylic acid 6-acryloyloxy-hexyl ester

Chemical Property:

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Technology Process of 4-{5-[4-(6-acryloyloxy-hexyloxy)-phenyl]-thiophen-2-yl}biphenyl-4-carboxylic acid 6-acryloyloxy-hexyl ester

There total 1 articles about 4-{5-[4-(6-acryloyloxy-hexyloxy)-phenyl]-thiophen-2-yl}biphenyl-4-carboxylic acid 6-acryloyloxy-hexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[5-(4-methoxyphenyl)thiophen-2-yl]boronic acid (666861-29-6) + 4-[5-(4-methoxyphenyl)-thiophen-2-yl]biphenyl-4-carboxylic acid methyl ester + 4-[5-(4-hydroxyphenyl)-thiophen-2-yl]biphenyl-4carboxylic acid → 4-{5-[4-(6-acryloyloxy-hexyloxy)-phenyl]-thiophen-2-yl}biphenyl-4-carboxylic acid 6-acryloyloxy-hexyl ester (666861-41-2)

Guidance literature:

[5-(4-methoxyphenyl)thiophen-2-yl]boronic acid; With methyl 4’-bromo-[1,1’-diphenyl]-4-carboxylate; potassium carbonate; tetrakis-(triphenylphosphino)-palladium⁽⁰⁾; In DMF (N,N-dimethyl-formamide); NaCl sol.; water; ethyl acetate; at 80 ℃; for 12h;

4-[5-(4-methoxyphenyl)-thiophen-2-yl]biphenyl-4-carboxylic acid methyl ester; 4-[5-(4-hydroxyphenyl)-thiophen-2-yl]biphenyl-4carboxylic acid; With acrylic acid 6-methanesulfonyloxy-hexyl ester; boron tribromide; potassium carbonate; more than 3 stages;

upstream raw materials:

[5-(4-methoxyphenyl)thiophen-2-yl]boronic acid