C₃₄H₅₂O₆Si

Base Information

• Chemical Name: C₃₄H₅₂O₆Si
• CAS No.: 939378-82-2
• Molecular Formula: C₃₄H₅₂O₆Si
• Molecular Weight: 584.869
• Mol file: 939378-82-2.mol

Synonyms:C₃₄H₅₂O₆Si

Chemical Property of C₃₄H₅₂O₆Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₄H₅₂O₆Si

There total 5 articles about C₃₄H₅₂O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C28H40O7Si (939378-65-1) + hexyltriphenylphosphonium bromide (4762-26-9) → C34H52O6Si (939378-82-2)

Guidance literature:

With sodium hexamethyldisilazane; In tetrahydrofuran; toluene; at -90 - 23 ℃;

DOI:10.1016/j.bmcl.2007.01.096

Reference yield:

C29H44O8Si → C34H52O6Si (939378-82-2)

Guidance literature:

Multi-step reaction with 2 steps

1: NaIO₄/SiO₂ / CH₂Cl₂ / 1.5 h / 23 °C

2: NaN(SiMe₃)2 / toluene; tetrahydrofuran / -90 - 23 °C

With sodium periodate; sodium hexamethyldisilazane; silica gel; In tetrahydrofuran; dichloromethane; toluene; 2: Wittig olefination;

DOI:10.1016/j.bmcl.2007.01.096

Reference yield:

C29H42O6Si (939378-81-1) → C34H52O6Si (939378-82-2)

Guidance literature:

Multi-step reaction with 3 steps

1: OsO₄; NMO / 2-methyl-propan-2-ol / 12 h / 23 °C

2: NaIO₄/SiO₂ / CH₂Cl₂ / 1.5 h / 23 °C

3: NaN(SiMe₃)2 / toluene; tetrahydrofuran / -90 - 23 °C

With sodium periodate; osmium(VIII) oxide; N-methyl-2-indolinone; sodium hexamethyldisilazane; silica gel; In tetrahydrofuran; dichloromethane; toluene; tert-butyl alcohol; 3: Wittig olefination;

DOI:10.1016/j.bmcl.2007.01.096

upstream raw materials:

C₂₈H₄₀O₇Si

hexyltriphenylphosphonium bromide

C₂₉H₄₂O₆Si

C₂₃H₂₈O₆

Downstream raw materials:

C₃₄H₅₄O₆Si

C₂₈H₄₀O₆

C₃₅H₄₄O₇