Technology Process of C22H20N4O
There total 5 articles about C22H20N4O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydrogencarbonate;
In
dichloromethane; water;
at 0 ℃;
for 15h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hydrogen / palladium 10% on activated carbon / ethanol / 15 h / 20 °C / 760.05 Torr
1.2: 3 h / 20 °C
2.1: potassium carbonate / methanol; water / 15 h / 60 °C
3.1: caesium carbonate / tetrahydrofuran / 15 h / Heating / reflux
4.1: hydrogenchloride / 1,4-dioxane; ethyl acetate / 20 °C
5.1: sodium hydrogencarbonate / dichloromethane; water / 15 h / 0 °C
With
hydrogenchloride; hydrogen; sodium hydrogencarbonate; potassium carbonate; caesium carbonate;
palladium 10% on activated carbon;
In
tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; water; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogenchloride / 1,4-dioxane; ethyl acetate / 20 °C
2: sodium hydrogencarbonate / dichloromethane; water / 15 h / 0 °C
With
hydrogenchloride; sodium hydrogencarbonate;
In
1,4-dioxane; dichloromethane; water; ethyl acetate;