[PdCl(triphenylphosphine)(κ²-C,N-1-methyl-2-phenylindole-3-azo-(4'-chlorobenzene)(-1H))]

Base Information

• Chemical Name: [PdCl(triphenylphosphine)(κ²-C,N-1-methyl-2-phenylindole-3-azo-(4'-chlorobenzene)(-1H))]
• CAS No.: 1422280-60-1
• Molecular Formula: C₃₉H₃₀Cl₂N₃PPd
• Molecular Weight: 748.987

Synonyms:[PdCl(triphenylphosphine)(κ²-C,N-1-methyl-2-phenylindole-3-azo-(4'-chlorobenzene)(-1H))]

Chemical Property of [PdCl(triphenylphosphine)(κ²-C,N-1-methyl-2-phenylindole-3-azo-(4'-chlorobenzene)(-1H))]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of [PdCl(triphenylphosphine)(κ²-C,N-1-methyl-2-phenylindole-3-azo-(4'-chlorobenzene)(-1H))]

There total 2 articles about [PdCl(triphenylphosphine)(κ²-C,N-1-methyl-2-phenylindole-3-azo-(4'-chlorobenzene)(-1H))] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

1-methyl-2-phenylindole-3-azo-(4'-chlorobenzene) (921753-83-5) + triphenylphosphine (603-35-0) + palladium dichloride → [PdCl(triphenylphosphine)(κ2-C,N-1-methyl-2-phenylindole-3-azo-(4'-chlorobenzene)(-1H))] (1422280-60-1)

Guidance literature:

1-methyl-2-phenylindole-3-azo-(4'-chlorobenzene); palladium dichloride; In methanol; dichloromethane; at 24.84 ℃; for 48h;

triphenylphosphine; In methanol; dichloromethane; at 24.84 ℃; for 24h;

DOI:10.1016/j.jorganchem.2012.11.036

Reference yield:

2-phenylindole-3-azo-(4'-chlorobenzene) (1422280-59-8) → [PdCl(triphenylphosphine)(κ2-C,N-1-methyl-2-phenylindole-3-azo-(4'-chlorobenzene)(-1H))] (1422280-60-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium hydroxide; Aliquat 336 / dichloromethane / 24 h / 24.84 °C

2.1: dichloromethane; methanol / 48 h / 24.84 °C

2.2: 24 h / 24.84 °C

With Aliquat 336; sodium hydroxide; In methanol; dichloromethane;

DOI:10.1016/j.jorganchem.2012.11.036

Reference yield: 95.0%

[PdCl(triphenylphosphine)(κ2-C,N-1-methyl-2-phenylindole-3-azo-(4'-chlorobenzene)(-1H))] (1422280-60-1) + triphenylphosphine (603-35-0) → trans-[PdCl(PPh3)2(κ1-C-1-methyl-2-phenylindole-3-azo-(4'-chlorobenzene)(-1H))]

Guidance literature:

In dichloromethane; at 24.84 ℃; for 2h;

DOI:10.1016/j.jorganchem.2012.11.036

upstream raw materials:

2-phenylindole-3-azo-(4'-chlorobenzene)

1-methyl-2-phenylindole-3-azo-(4'-chlorobenzene)

triphenylphosphine

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