exo-2-(3,5-Dimethoxybenzoyloxy)-8,8-dimethyl-1-azabicyclo<3.2.1>oct-6-en

Base Information

Chemical Name:exo-2-(3,5-Dimethoxybenzoyloxy)-8,8-dimethyl-1-azabicyclo<3.2.1>oct-6-en
CAS No.:109638-38-2
Molecular Formula:C₁₈H₂₃NO₄
Molecular Weight:317.385
Hs Code.:

Synonyms:exo-2-(3,5-Dimethoxybenzoyloxy)-8,8-dimethyl-1-azabicyclo<3.2.1>oct-6-en

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Chemical Property of exo-2-(3,5-Dimethoxybenzoyloxy)-8,8-dimethyl-1-azabicyclo<3.2.1>oct-6-en

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Technology Process of exo-2-(3,5-Dimethoxybenzoyloxy)-8,8-dimethyl-1-azabicyclo<3.2.1>oct-6-en

There total 6 articles about exo-2-(3,5-Dimethoxybenzoyloxy)-8,8-dimethyl-1-azabicyclo<3.2.1>oct-6-en which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 109638-22-4
2-(3,5-Dimethoxybenzoyloxy)-3,3-dimethyl-2-azabicyclo<2.2.2>oct-5-en

: 1132-21-4
3,5-dimethoxybenzoic acid

: 109638-38-2
exo-2-(3,5-Dimethoxybenzoyloxy)-8,8-dimethyl-1-azabicyclo<3.2.1>oct-6-en

: 109638-26-8
2-(3,5-Dimethoxybenzoyl)-3,3-dimethyl-2-azabicyclo<2.2.2>oct-5-en

Guidance literature:: In toluene; for 48h; Heating;

Reference yield:

: 109638-18-8
3,3-Dimethyl-2-nitroso-2-azabicyclo<2.2.2>oct-5-en

: 109638-38-2
exo-2-(3,5-Dimethoxybenzoyloxy)-8,8-dimethyl-1-azabicyclo<3.2.1>oct-6-en

Guidance literature:: Multi-step reaction with 5 steps

1: 76 percent / HCl-gas / diethyl ether / 2 h

2: 1) conc. NaOH; NaHCO₃, Na₂WO₄, 2) H₂O₂ / 1) CH₃OH, CH₃CN, 2) 15 h, 0 deg C; 3 d, 20 deg C

3: LiAlH₄ / 1) 30 min, 20 deg C, 2) 15 min, reflux

4: NaOH / CH₂Cl₂ / 0.33 h / 20 °C

5: 2.6 percent / toluene / 48 h / Heating

With hydrogenchloride; sodium hydroxide; sodium tungstate; lithium aluminium tetrahydride; dihydrogen peroxide; sodium hydrogencarbonate; In diethyl ether; dichloromethane; toluene;

Reference yield:

: 109638-19-9
3,3-Dimethyl-2-azabicyclo<2.2.2>oct-5-en-hydrochlorid

: 109638-38-2
exo-2-(3,5-Dimethoxybenzoyloxy)-8,8-dimethyl-1-azabicyclo<3.2.1>oct-6-en

Guidance literature:: Multi-step reaction with 4 steps

1: 1) conc. NaOH; NaHCO₃, Na₂WO₄, 2) H₂O₂ / 1) CH₃OH, CH₃CN, 2) 15 h, 0 deg C; 3 d, 20 deg C

2: LiAlH₄ / 1) 30 min, 20 deg C, 2) 15 min, reflux

3: NaOH / CH₂Cl₂ / 0.33 h / 20 °C

4: 2.6 percent / toluene / 48 h / Heating

With sodium hydroxide; sodium tungstate; lithium aluminium tetrahydride; dihydrogen peroxide; sodium hydrogencarbonate; In dichloromethane; toluene;