6-O-acetyl-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate

Base Information

Chemical Name:6-O-acetyl-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate
CAS No.:346441-49-4
Molecular Formula:C₃₁H₂₆Cl₃NO₁₀
Molecular Weight:678.907
Hs Code.:

Synonyms:6-O-acetyl-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate

Suppliers and Price of 6-O-acetyl-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemicals and raw materials
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Total 3 raw suppliers

Chemical Property of 6-O-acetyl-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of 6-O-acetyl-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate

There total 3 articles about 6-O-acetyl-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.1%

: 545-06-2
trichloroacetonitrile

: 346441-48-3
6-O-acetyl-2,3,4-tri-O-benzoyl-α-D-mannopyranose

: 346441-49-4
6-O-acetyl-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In diethyl ether; at 0 ℃; for 2h;
DOI:10.1016/S0008-6215(01)00059-3

Reference yield:

: 545-06-2
trichloroacetonitrile

: 6-O-acetyl-2,3,4-tri-O-benzoyl-D-mannopyranose

: 346441-49-4
6-O-acetyl-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1016/j.carres.2004.01.020

Reference yield:

: 346441-47-2
1,6-di-O-acetyl-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

: 346441-49-4
6-O-acetyl-2,3,4-tri-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 2 steps

1: NH₃ / methanol; tetrahydrofuran / 0.75 h

2: 1.47 g / DBU / CH₂Cl₂ / 2 h / 20 °C

With ammonia; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.carres.2004.01.020