H-Glu(Bzl)-Asp(Bzl)-Met-Glu(Bzl)-Tyr(Bzl)-OMe trifluoroacetic salt

Base Information

Chemical Name:H-Glu(Bzl)-Asp(Bzl)-Met-Glu(Bzl)-Tyr(Bzl)-OMe trifluoroacetic salt
CAS No.:104945-76-8
Molecular Formula:C₂HF₃O₂*C₅₇H₆₅N₅O₁₃S
Molecular Weight:1174.26
Hs Code.:

Synonyms:H-Glu(Bzl)-Asp(Bzl)-Met-Glu(Bzl)-Tyr(Bzl)-OMe trifluoroacetic salt

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Chemical Property of H-Glu(Bzl)-Asp(Bzl)-Met-Glu(Bzl)-Tyr(Bzl)-OMe trifluoroacetic salt

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Technology Process of H-Glu(Bzl)-Asp(Bzl)-Met-Glu(Bzl)-Tyr(Bzl)-OMe trifluoroacetic salt

There total 4 articles about H-Glu(Bzl)-Asp(Bzl)-Met-Glu(Bzl)-Tyr(Bzl)-OMe trifluoroacetic salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 104945-74-6
Boc-Glu(Bzl)-Asp(Bzl)-Met-Glu(Bzl)-Tyr(Bzl)-OMe

: 76-05-1
trifluoroacetic acid

: 104945-76-8
H-Glu(Bzl)-Asp(Bzl)-Met-Glu(Bzl)-Tyr(Bzl)-OMe trifluoroacetic salt

Guidance literature:: With p-cresol; phenol;

Reference yield:

: 1676-73-9,25014-27-1
L-glutamic acid γ-benzyl ester

: 104945-76-8
H-Glu(Bzl)-Asp(Bzl)-Met-Glu(Bzl)-Tyr(Bzl)-OMe trifluoroacetic salt

Guidance literature:: Multi-step reaction with 4 steps

1: 2-methyl-propan-2-ol; H₂O / pH 9.5-10.0

2: DCC / CH₂Cl₂; dimethylformamide / 1.25 h / 0 °C

3: 97 percent / N-methylmorpholine / CH₂Cl₂; dimethylformamide / 1.) 0 deg C, 2 h, 2.) 20 deg C, 2 h

4: 100 percent / p-cresol, PhOH

With 4-methyl-morpholine; p-cresol; dicyclohexyl-carbodiimide; phenol; In dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;

Reference yield:

: 13574-13-5
Boc-Glu(OBzl)-OH

: 104945-76-8
H-Glu(Bzl)-Asp(Bzl)-Met-Glu(Bzl)-Tyr(Bzl)-OMe trifluoroacetic salt

Guidance literature:: Multi-step reaction with 3 steps

1: DCC / CH₂Cl₂; dimethylformamide / 1.25 h / 0 °C

2: 97 percent / N-methylmorpholine / CH₂Cl₂; dimethylformamide / 1.) 0 deg C, 2 h, 2.) 20 deg C, 2 h

3: 100 percent / p-cresol, PhOH

With 4-methyl-morpholine; p-cresol; dicyclohexyl-carbodiimide; phenol; In dichloromethane; N,N-dimethyl-formamide;