N,N'-bis(1-benzyl-1H-[1,2,3]triazol-4-ylmethyl)-N,N'-dimethylethane-1,2-diamine

Base Information

• Chemical Name: N,N'-bis(1-benzyl-1H-[1,2,3]triazol-4-ylmethyl)-N,N'-dimethylethane-1,2-diamine
• CAS No.: 1519012-38-4
• Molecular Formula: C₂₄H₃₀N₈
• Molecular Weight: 430.556
• Mol file: 1519012-38-4.mol

Synonyms:N,N'-bis(1-benzyl-1H-[1,2,3]triazol-4-ylmethyl)-N,N'-dimethylethane-1,2-diamine

Chemical Property of N,N'-bis(1-benzyl-1H-[1,2,3]triazol-4-ylmethyl)-N,N'-dimethylethane-1,2-diamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N'-bis(1-benzyl-1H-[1,2,3]triazol-4-ylmethyl)-N,N'-dimethylethane-1,2-diamine

There total 1 articles about N,N'-bis(1-benzyl-1H-[1,2,3]triazol-4-ylmethyl)-N,N'-dimethylethane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

propargyl bromide (106-96-7) + benzyl azide (622-79-7) + N,N`-dimethylethylenediamine (110-70-3) → N,N'-bis(1-benzyl-1H-[1,2,3]triazol-4-ylmethyl)-N,N'-dimethylethane-1,2-diamine (1519012-38-4)

Guidance literature:

propargyl bromide; N,N`-dimethylethylenediamine; With triethylamine; In water; toluene; acetonitrile; at 20 ℃; for 1.5h; Inert atmosphere;

benzyl azide; With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; toluene; acetonitrile; at 20 ℃; Inert atmosphere;

DOI:10.1039/c3nj00570d

Reference yield: 75.0%

copper(II) perchlorate hexahydrate + N,N'-bis(1-benzyl-1H-[1,2,3]triazol-4-ylmethyl)-N,N'-dimethylethane-1,2-diamine (1519012-38-4) + acetonitrile (75-05-8,26809-02-9) → [Cu(N,N'-bis(1-benzyl-1H-[1,2,3]triazol-4-ylmethyl)-N,N'-dimethylethane-1,2-diamine)(MeCN)](ClO4)2

Guidance literature:

In ethanol; water; at 70 ℃; for 2h;

DOI:10.1039/c3nj00570d

upstream raw materials:

propargyl bromide

benzyl azide

N,N`-dimethylethylenediamine