di-tert-butyl 1-(1-benzoyl-4-oxopiperidin-3-yl)hydrazine-1,2-dicarboxylate

Base Information

Chemical Name:di-tert-butyl 1-(1-benzoyl-4-oxopiperidin-3-yl)hydrazine-1,2-dicarboxylate
CAS No.:1385032-99-4
Molecular Formula:C₂₂H₃₁N₃O₆
Molecular Weight:433.505
Hs Code.:

Synonyms:di-tert-butyl 1-(1-benzoyl-4-oxopiperidin-3-yl)hydrazine-1,2-dicarboxylate

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Chemical Property of di-tert-butyl 1-(1-benzoyl-4-oxopiperidin-3-yl)hydrazine-1,2-dicarboxylate

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Technology Process of di-tert-butyl 1-(1-benzoyl-4-oxopiperidin-3-yl)hydrazine-1,2-dicarboxylate

There total 1 articles about di-tert-butyl 1-(1-benzoyl-4-oxopiperidin-3-yl)hydrazine-1,2-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 24686-78-0
1-Benzoyl-4-piperidone

: 870-50-8
di-tert-butyl-diazodicarboxylate

: 1385032-99-4
di-tert-butyl 1-(1-benzoyl-4-oxopiperidin-3-yl)hydrazine-1,2-dicarboxylate

: 1385033-09-9
tetra-tert-butyl 1,1'-(1-benzoyl-4-oxopiperidine-3,5-diyl)di(hydrazine-1,2-dicarboxylate)

Guidance literature:: With L-proline; In acetonitrile; at 0 - 20 ℃; for 25h;
DOI:10.1007/s10593-012-0993-3

Reference yield:

: 1385032-99-4
di-tert-butyl 1-(1-benzoyl-4-oxopiperidin-3-yl)hydrazine-1,2-dicarboxylate

: 1385033-04-4
1-benzoyl-3-(1H-pyrazol-1-yl)piperidin-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / ethanol; water / 4 h

2: ethanol; water / 3 h / Reflux

With hydrogenchloride; In ethanol; water;
DOI:10.1007/s10593-012-0993-3