Technology Process of C43H53N7O8
There total 13 articles about C43H53N7O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C43H51N7O9;
With
calcium borohydride bis(tetrahydrofuran);
In
tetrahydrofuran;
at 0 - 23 ℃;
for 0.5h;
With
sodium cyanoborohydride; acetic acid;
at 0 - 50 ℃;
for 0.5h;
DOI:10.1039/c0cc02214d
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: Dess-Martin periodane / dichloromethane; water / 2 h / 23 °C
2.1: manganese(III) triacetate dihydrate; acetic acid / 0 - 60 °C / Inert atmosphere
3.1: lithium hydroxide / tetrahydrofuran; water / 0.5 h / 23 °C
3.2: 0 - 23 °C / Inert atmosphere
4.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 - 0 °C
5.1: calcium borohydride bis(tetrahydrofuran) / tetrahydrofuran / 0.5 h / 0 - 23 °C
5.2: 0.5 h / 0 - 50 °C
With
calcium borohydride bis(tetrahydrofuran); manganese(III) triacetate dihydrate; Dess-Martin periodane; acetic acid; lithium hydroxide; lithium hexamethyldisilazane;
In
tetrahydrofuran; dichloromethane; water;
3.2: Mitsunobu reaction;
DOI:10.1039/c0cc02214d
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 - 0 °C
2.1: calcium borohydride bis(tetrahydrofuran) / tetrahydrofuran / 0.5 h / 0 - 23 °C
2.2: 0.5 h / 0 - 50 °C
With
calcium borohydride bis(tetrahydrofuran); lithium hexamethyldisilazane;
In
tetrahydrofuran;
DOI:10.1039/c0cc02214d
