5-oxo-5-(3,4-bishexyloxy)phenyl pentanoic acid methyl ester tosyl hydrazone

Base Information

• Chemical Name: 5-oxo-5-(3,4-bishexyloxy)phenyl pentanoic acid methyl ester tosyl hydrazone
• CAS No.: 340734-84-1
• Molecular Formula: C₃₁H₄₆N₂O₆S
• Molecular Weight: 574.782
• Mol file: 340734-84-1.mol

Synonyms:5-oxo-5-(3,4-bishexyloxy)phenyl pentanoic acid methyl ester tosyl hydrazone

Chemical Property of 5-oxo-5-(3,4-bishexyloxy)phenyl pentanoic acid methyl ester tosyl hydrazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-oxo-5-(3,4-bishexyloxy)phenyl pentanoic acid methyl ester tosyl hydrazone

There total 3 articles about 5-oxo-5-(3,4-bishexyloxy)phenyl pentanoic acid methyl ester tosyl hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

toluene-4-sulfonic acid hydrazide (1576-35-8) + 5-oxo-5-(3,4-bishexyloxy)phenyl pentanoic acid methyl ester → 5-oxo-5-(3,4-bishexyloxy)phenyl pentanoic acid methyl ester tosyl hydrazone (340734-84-1)

Guidance literature:

In methanol; for 5.5h; Heating;

DOI:10.1039/b008006n

Reference yield:

methyl 4-(chlorocarbonyl)butyrate (1501-26-4) → 5-oxo-5-(3,4-bishexyloxy)phenyl pentanoic acid methyl ester tosyl hydrazone (340734-84-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 72 percent / aluminum trichloride / CS₂ / 20 - 35 °C

2: 61 percent / methanol / 5.5 h / Heating

With aluminium trichloride; In methanol; carbon disulfide;

DOI:10.1039/b008006n

Reference yield:

1,2-dihexyloxybenzene (94259-20-8) → 5-oxo-5-(3,4-bishexyloxy)phenyl pentanoic acid methyl ester tosyl hydrazone (340734-84-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 72 percent / aluminum trichloride / CS₂ / 20 - 35 °C

2: 61 percent / methanol / 5.5 h / Heating

With aluminium trichloride; In methanol; carbon disulfide;

DOI:10.1039/b008006n

upstream raw materials:

toluene-4-sulfonic acid hydrazide

methyl 4-(chlorocarbonyl)butyrate

1,2-dihexyloxybenzene

Downstream raw materials:

C₈₄H₃₈O₄