(R)-tert-butyl 5-(2-(benzyl(2-hydroxyethyl)amino)-1-(triethylsilyloxy)ethyl)-2-chlorophenyl(methylsulfonyl)carbamate

Base Information

• Chemical Name: (R)-tert-butyl 5-(2-(benzyl(2-hydroxyethyl)amino)-1-(triethylsilyloxy)ethyl)-2-chlorophenyl(methylsulfonyl)carbamate
• CAS No.: 1221179-17-4
• Molecular Formula: C₂₉H₄₅ClN₂O₆SSi
• Molecular Weight: 613.291

Synonyms:(R)-tert-butyl 5-(2-(benzyl(2-hydroxyethyl)amino)-1-(triethylsilyloxy)ethyl)-2-chlorophenyl(methylsulfonyl)carbamate

Chemical Property of (R)-tert-butyl 5-(2-(benzyl(2-hydroxyethyl)amino)-1-(triethylsilyloxy)ethyl)-2-chlorophenyl(methylsulfonyl)carbamate

Chemical Property:

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Technology Process of (R)-tert-butyl 5-(2-(benzyl(2-hydroxyethyl)amino)-1-(triethylsilyloxy)ethyl)-2-chlorophenyl(methylsulfonyl)carbamate

There total 1 articles about (R)-tert-butyl 5-(2-(benzyl(2-hydroxyethyl)amino)-1-(triethylsilyloxy)ethyl)-2-chlorophenyl(methylsulfonyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) + (R)-N-(5-(2-(Benzyl(2-hydroxyethyl)amino)-1-(triethylsilyloxy)ethyl)-2-chlorophenyl)methanesulfonamide (1221179-16-3) → (R)-tert-butyl 5-(2-(benzyl(2-hydroxyethyl)amino)-1-(triethylsilyloxy)ethyl)-2-chlorophenyl(methylsulfonyl)carbamate (1221179-17-4)

Guidance literature:

With dmap; triethylamine; In tetrahydrofuran; at 0 - 20 ℃;

Reference yield:

tert-butyl 3-cyclobutyl-6-hydroxy-1H-indazole-1-carboxylate (1221235-58-0) + (R)-tert-butyl 5-(2-(benzyl(2-hydroxyethyl)amino)-1-(triethylsilyloxy)ethyl)-2-chlorophenyl(methylsulfonyl)carbamate (1221179-17-4) → (R)-tert-butyl 6-(2-(benzyl(2-(3-(N-(tert-butoxycarbonyl)methylsulfonamide)-4-chlorophenyl)-2-(triethylsilyloxy)ethyl)amino)ethoxy)-3-cyclobutylindazole-1-carboxylate (1221235-74-0)

Guidance literature:

With diamide; triphenylphosphine; In toluene; at 20 ℃; for 72h;

Reference yield:

tert-butyl 3-ethyl-6-hydroxy-1H-indazole-1-carboxylate (1221178-64-8) + (R)-tert-butyl 5-(2-(benzyl(2-hydroxyethyl)amino)-1-(triethylsilyloxy)ethyl)-2-chlorophenyl(methylsulfonyl)carbamate (1221179-17-4) → (R)-tert-butyl 6-(2-(benzyl-(2-(3-(N-(tert-butoxycarbonyl)(methyl)sulfonamido)-4-chlorophenyl)-2-(triethylsilyloxy)ethyl)amino)ethoxy)-3-ethylindazole-1-carboxylate (1221179-18-5)

Guidance literature:

With diamide; triphenylphosphine; In toluene; at 20 ℃; for 72h;

upstream raw materials:

di-tert-butyl dicarbonate

(R)-N-(5-(2-(Benzyl(2-hydroxyethyl)amino)-1-(triethylsilyloxy)ethyl)-2-chlorophenyl)methanesulfonamide

Downstream raw materials:

(R)-tert-butyl 6-(2-(benzyl(2-(3-(N-(tert-butoxycarbonyl)methylsulfonamide)-4-chlorophenyl)-2-(triethylsilyloxy)ethyl)amino)ethoxy)-3-cyclobutylindazole-1-carboxylate

(R)-tert-butyl 6-(2-(benzyl-(2-(3-(N-(tert-butoxycarbonyl)(methyl)sulfonamido)-4-chlorophenyl)-2-(triethylsilyloxy)ethyl)amino)ethoxy)-3-ethylindazole-1-carboxylate

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