C₃₇H₄₄N₂O₈Si

Base Information

Chemical Name:C₃₇H₄₄N₂O₈Si
CAS No.:1616784-15-6
Molecular Formula:C₃₇H₄₄N₂O₈Si
Molecular Weight:672.85
Hs Code.:

C<sub>37</sub>H<sub>44</sub>N<sub>2</sub>O<sub>8</sub>Si

Synonyms:C₃₇H₄₄N₂O₈Si

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Chemical Property of C₃₇H₄₄N₂O₈Si

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Technology Process of C₃₇H₄₄N₂O₈Si

There total 5 articles about C₃₇H₄₄N₂O₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1616784-14-5
C₃₇H₄₄N₂O₇Si

: 1616784-15-6
C₃₇H₄₄N₂O₈Si

Guidance literature:: With sodium dihydrogenphosphate; 2-methyl-but-2-ene; sodium perchlorate; In tetrahydrofuran; water; tert-butyl alcohol; at 20 ℃; for 1h;
DOI:10.1093/nar/gku235 DOI:10.1093/nar/gku669

Reference yield:

: 200011-14-9
1-[3-C-allyl-2,5-O-bis(tert-butyldimethylsilyl)-β-D-pentofuranosyl]-uracyl

: 1616784-15-6
C₃₇H₄₄N₂O₈Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: trifluoroacetic acid / tetrahydrofuran; water / 4 h / 0 °C

2.1: pyridine / 14 h / 0 - 20 °C

3.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / 1,4-dioxane / 10 h / 20 °C

3.2: 12 h / 20 °C

4.1: sodium perchlorate; sodium dihydrogenphosphate; 2-methyl-but-2-ene / tetrahydrofuran; water; tert-butyl alcohol / 1 h / 20 °C

With pyridine; sodium dihydrogenphosphate; osmium(VIII) oxide; 2-methyl-but-2-ene; sodium perchlorate; 4-methylmorpholine N-oxide; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; water; tert-butyl alcohol;
DOI:10.1093/nar/gku235

Reference yield:

: 1616784-12-3
C₁₈H₃₀N₂O₅Si

: 1616784-15-6
C₃₇H₄₄N₂O₈Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine / 14 h / 0 - 20 °C

2.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / 1,4-dioxane / 10 h / 20 °C

2.2: 12 h / 20 °C

3.1: sodium perchlorate; sodium dihydrogenphosphate; 2-methyl-but-2-ene / tetrahydrofuran; water; tert-butyl alcohol / 1 h / 20 °C

With pyridine; sodium dihydrogenphosphate; osmium(VIII) oxide; 2-methyl-but-2-ene; sodium perchlorate; 4-methylmorpholine N-oxide; In tetrahydrofuran; 1,4-dioxane; water; tert-butyl alcohol;
DOI:10.1093/nar/gku235