C₂₃H₃₀O₂Se

Base Information

• Chemical Name: C₂₃H₃₀O₂Se
• CAS No.: 1160556-71-7
• Molecular Formula: C₂₃H₃₀O₂Se
• Molecular Weight: 417.45
• Mol file: 1160556-71-7.mol

Synonyms:C₂₃H₃₀O₂Se

Chemical Property of C₂₃H₃₀O₂Se

Chemical Property:

Purity/Quality:

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Technology Process of C₂₃H₃₀O₂Se

There total 1 articles about C₂₃H₃₀O₂Se which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

C15H22OSe (1160556-77-3) + p-methoxybenzyl chloride (824-94-2) → C23H30O2Se (1160556-71-7)

Guidance literature:

C₁₅H₂₂OSe; With sodium hydride; In tetrahydrofuran; dimethyl sulfoxide; mineral oil; at 0 ℃; for 0.166667h;

p-methoxybenzyl chloride; With tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; dimethyl sulfoxide; mineral oil; at 0 - 23 ℃; for 17h;

DOI:10.1021/ol900819u

Reference yield: 86.0%

C23H30O2Se (1160556-71-7) + C19H35IO3Si (1160556-74-0) → C42H66O5SeSi (1160556-78-4)

Guidance literature:

C₂₃H₃₀O₂Se; With 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; at 40 ℃; for 24h; Inert atmosphere;

C₁₉H₃₅IO₃Si; With triphenyl-arsane; caesium carbonate; In tetrahydrofuran; water; N,N-dimethyl-formamide; for 0.0833333h; Inert atmosphere;

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In tetrahydrofuran; water; N,N-dimethyl-formamide; at 80 ℃; for 8h; Inert atmosphere;

DOI:10.1021/ol900819u

upstream raw materials:

C₁₅H₂₂OSe

p-methoxybenzyl chloride

Downstream raw materials:

C₄₂H₆₆O₅SeSi