1,3-bis<<<6-(3-(benzoylmercapto)propionylamino)pyrid-2-yl>amino>carbonyl>-5-(heptyloxy)benzene

Base Information

• Chemical Name: 1,3-bis<<<6-(3-(benzoylmercapto)propionylamino)pyrid-2-yl>amino>carbonyl>-5-(heptyloxy)benzene
• CAS No.: 162968-34-5
• Molecular Formula: C₄₅H₄₆N₆O₇S₂
• Molecular Weight: 847.028

Synonyms:1,3-bis<<<6-(3-(benzoylmercapto)propionylamino)pyrid-2-yl>amino>carbonyl>-5-(heptyloxy)benzene

Chemical Property of 1,3-bis<<<6-(3-(benzoylmercapto)propionylamino)pyrid-2-yl>amino>carbonyl>-5-(heptyloxy)benzene

Chemical Property:

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Technology Process of 1,3-bis<<<6-(3-(benzoylmercapto)propionylamino)pyrid-2-yl>amino>carbonyl>-5-(heptyloxy)benzene

There total 2 articles about 1,3-bis<<<6-(3-(benzoylmercapto)propionylamino)pyrid-2-yl>amino>carbonyl>-5-(heptyloxy)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-benzoylthiopropanoic acid (60718-18-5) → 1,3-bis<<<6-(3-(benzoylmercapto)propionylamino)pyrid-2-yl>amino>carbonyl>-5-(heptyloxy)benzene (162968-34-5)

Guidance literature:

Multi-step reaction with 2 steps

1: (COCl)2, DMF / CH₂Cl₂ / Ambient temperature

2: Et₃N / tetrahydrofuran / Ambient temperature

With oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane;

DOI:10.1016/0040-4020(94)00907-C

Reference yield:

S-benzoyl-3-mercaptopropanoyl chloride (67714-30-1) + 1,3-bis<<(6-aminopyrid-2-yl)amino>carbonyl>-5-(heptyloxy)benzene (129648-67-5) → 1,3-bis<<<6-(3-(benzoylmercapto)propionylamino)pyrid-2-yl>amino>carbonyl>-5-(heptyloxy)benzene (162968-34-5)

Guidance literature:

With triethylamine; In tetrahydrofuran; Yield given; Ambient temperature;

DOI:10.1016/0040-4020(94)00907-C

Reference yield: 66.0%

1,3-bis<<<6-(3-(benzoylmercapto)propionylamino)pyrid-2-yl>amino>carbonyl>-5-(heptyloxy)benzene (162968-34-5) → 1,3-bis<<<6-(3-mercaptopropionylamino)pyrid-2-yl>amino>carbonyl>-5-(heptyloxy)benzene

Guidance literature:

With sodium hydroxide; In methanol; dichloromethane; for 1h; Ambient temperature;

DOI:10.1016/0040-4020(94)00907-C

upstream raw materials:

S-benzoyl-3-mercaptopropanoyl chloride

1,3-bis<<(6-aminopyrid-2-yl)amino>carbonyl>-5-(heptyloxy)benzene

3-benzoylthiopropanoic acid

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