Ethyl 2-O-benzoyl-4-O-benzyl-6-O-tert-butyldiphenylsilyl-1-thio-α-D-glucopyranoside

Base Information

Chemical Name:Ethyl 2-O-benzoyl-4-O-benzyl-6-O-tert-butyldiphenylsilyl-1-thio-α-D-glucopyranoside
CAS No.:162316-88-3
Molecular Formula:C₃₈H₄₄O₆SSi
Molecular Weight:656.915
Hs Code.:

Synonyms:Ethyl 2-O-benzoyl-4-O-benzyl-6-O-tert-butyldiphenylsilyl-1-thio-α-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethyl 2-O-benzoyl-4-O-benzyl-6-O-tert-butyldiphenylsilyl-1-thio-α-D-glucopyranoside

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Technology Process of Ethyl 2-O-benzoyl-4-O-benzyl-6-O-tert-butyldiphenylsilyl-1-thio-α-D-glucopyranoside

There total 8 articles about Ethyl 2-O-benzoyl-4-O-benzyl-6-O-tert-butyldiphenylsilyl-1-thio-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 473545-19-6
ethyl 2-O-benzoyl-4-O-benzyl-1-thio-α-D-glucopyranoside

: 162316-88-3
Ethyl 2-O-benzoyl-4-O-benzyl-6-O-tert-butyldiphenylsilyl-1-thio-α-D-glucopyranoside

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 3h;
DOI:10.1246/bcsj.76.1829

Reference yield: 84.0%

: 54769-36-7
N-benzoyloxybenzotriazole

: 162316-87-2
Ethyl 4-O-benzyl-6-O-tert-butyldiphenylsilyl-1-thio-α-D-glucopyranoside

: 162316-88-3
Ethyl 2-O-benzoyl-4-O-benzyl-6-O-tert-butyldiphenylsilyl-1-thio-α-D-glucopyranoside

Guidance literature:: With triethylamine; In dichloromethane; Ambient temperature;

Reference yield:

: 151123-94-3
Ethyl 2-O-benzoyl-4,6-O-benzylidene-3-O-chloroacetyl-1-thio-α-D-glucopyranoside

: 162316-88-3
Ethyl 2-O-benzoyl-4-O-benzyl-6-O-tert-butyldiphenylsilyl-1-thio-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 57 percent / triethylamine-borane; AlCl₃ / CH₂Cl₂; diethyl ether / 0.5 h / 20 °C

2: 43 percent / thiourea / dimethylformamide / 3 h / 70 °C

3: 100 percent / imidazole / dimethylformamide / 3 h / 20 °C

With 1H-imidazole; aluminium trichloride; triethylamine borane; thiourea; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.76.1829