7-isopropoxy-2-[methoxy-2-(4-methoxyphenyl)ethenyl]-3-{4-(4-methoxyphenyl)-1-[2-(4-methoxyphenyl)ethyl]-1H-pyrrol-3-yl}-1H-indole

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Chemical Name:7-isopropoxy-2-[methoxy-2-(4-methoxyphenyl)ethenyl]-3-{4-(4-methoxyphenyl)-1-[2-(4-methoxyphenyl)ethyl]-1H-pyrrol-3-yl}-1H-indole
CAS No.:864816-23-9
Molecular Formula:C₄₁H₄₂N₂O₅
Molecular Weight:642.795
Hs Code.:

Synonyms:7-isopropoxy-2-[methoxy-2-(4-methoxyphenyl)ethenyl]-3-{4-(4-methoxyphenyl)-1-[2-(4-methoxyphenyl)ethyl]-1H-pyrrol-3-yl}-1H-indole

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Chemical Property of 7-isopropoxy-2-[methoxy-2-(4-methoxyphenyl)ethenyl]-3-{4-(4-methoxyphenyl)-1-[2-(4-methoxyphenyl)ethyl]-1H-pyrrol-3-yl}-1H-indole

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Technology Process of 7-isopropoxy-2-[methoxy-2-(4-methoxyphenyl)ethenyl]-3-{4-(4-methoxyphenyl)-1-[2-(4-methoxyphenyl)ethyl]-1H-pyrrol-3-yl}-1H-indole

There total 12 articles about 7-isopropoxy-2-[methoxy-2-(4-methoxyphenyl)ethenyl]-3-{4-(4-methoxyphenyl)-1-[2-(4-methoxyphenyl)ethyl]-1H-pyrrol-3-yl}-1H-indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 864816-22-8
2-N-[2-isopropoxy-6-({4-(4-methoxyphenyl)-1-[2-(4-methoxyphenyl)ethyl]-1H-pyrrol-3-yl}carbonyl)phenyl]-2-methoxy-3-(4-methoxyphenyl)-2-propenamide

: 864816-23-9
7-isopropoxy-2-[methoxy-2-(4-methoxyphenyl)ethenyl]-3-{4-(4-methoxyphenyl)-1-[2-(4-methoxyphenyl)ethyl]-1H-pyrrol-3-yl}-1H-indole

Guidance literature:: With pyridine; titanium(III) chloride; potassium graphite; In 1,2-dimethoxyethane; for 1.5h; Heating;
DOI:10.1021/ja0541175

Reference yield:

: 864816-17-1
3-isopropoxy-2-nitrophenylethanone

: 864816-23-9
7-isopropoxy-2-[methoxy-2-(4-methoxyphenyl)ethenyl]-3-{4-(4-methoxyphenyl)-1-[2-(4-methoxyphenyl)ethyl]-1H-pyrrol-3-yl}-1H-indole

Guidance literature:: Multi-step reaction with 5 steps

1.1: 74 percent / sodium / methanol / 2 h / 70 °C

2.1: NaH / tetrahydrofuran / 3 h / -30 - 20 °C

2.2: 83 percent / tetrahydrofuran / 2 h / Heating

3.1: 96 percent / aq. HCl; iron / ethanol / 2 h / Heating

4.1: 89 percent / Et₃N; DMAP / CH₂Cl₂ / 0.5 h / 20 °C

5.1: 93 percent / C₈K; TiCl₃; pyridine / 1,2-dimethoxy-ethane / 1.5 h / Heating

With pyridine; hydrogenchloride; dmap; titanium(III) chloride; sodium; iron; sodium hydride; triethylamine; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; ethanol; dichloromethane;
DOI:10.1021/ja0617800

Reference yield:

: 864816-21-7
(Z)-2-Methoxy-3-(4-methoxy-phenyl)-acryloyl chloride

: 864816-23-9
7-isopropoxy-2-[methoxy-2-(4-methoxyphenyl)ethenyl]-3-{4-(4-methoxyphenyl)-1-[2-(4-methoxyphenyl)ethyl]-1H-pyrrol-3-yl}-1H-indole

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / Et₃N; DMAP / CH₂Cl₂ / 0.5 h / 20 °C

2: 93 percent / C₈K; TiCl₃; pyridine / 1,2-dimethoxy-ethane / 1.5 h / Heating

With pyridine; dmap; titanium(III) chloride; triethylamine; In 1,2-dimethoxyethane; dichloromethane;
DOI:10.1021/ja0617800