2,4-di-tert-butylphenoxyferrocene

Base Information

• Chemical Name: 2,4-di-tert-butylphenoxyferrocene
• CAS No.: 704898-65-7
• Molecular Formula: C₂₄H₃₀FeO
• Molecular Weight: 390.349
• Mol file: 704898-65-7.mol

Synonyms:2,4-di-tert-butylphenoxyferrocene

Chemical Property of 2,4-di-tert-butylphenoxyferrocene

Chemical Property:

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Technology Process of 2,4-di-tert-butylphenoxyferrocene

There total 1 articles about 2,4-di-tert-butylphenoxyferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

iodoferrocene (1273-76-3) + 2,4-di-tert-Butylphenol (96-76-4) → 2,4-di-tert-butylphenoxyferrocene (704898-65-7)

Guidance literature:

With caesium carbonate; In further solvent(s); under Ar; CuI, 2,2,6,6-tetramethylheptane-3,5-dione, Fe complex, phenol and Cs2CO3 (0.05:0.12:1:2:2) dissolved in NMP; stirred at 110°C for 20 h; Et2O added; extd. with water; solvent evapd.; purified by column chromy.(silica, n-heptane);

DOI:10.1021/om0497893

upstream raw materials:

iodoferrocene

2,4-di-tert-Butylphenol