2-cyano-2-(1-ethoxyethoxy)-1-<3,5-bis(benzyloxy)-2-methyl-4-<(2)H3>methylphenyl>propane

Base Information

Chemical Name:2-cyano-2-(1-ethoxyethoxy)-1-<3,5-bis(benzyloxy)-2-methyl-4-<(2)H3>methylphenyl>propane
CAS No.:89505-66-8
Molecular Formula:C₃₀H₃₅NO₄
Molecular Weight:476.588
Hs Code.:

Synonyms:2-cyano-2-(1-ethoxyethoxy)-1-<3,5-bis(benzyloxy)-2-methyl-4-<(2)H3>methylphenyl>propane

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Chemical Property of 2-cyano-2-(1-ethoxyethoxy)-1-<3,5-bis(benzyloxy)-2-methyl-4-<(2)H3>methylphenyl>propane

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Technology Process of 2-cyano-2-(1-ethoxyethoxy)-1-<3,5-bis(benzyloxy)-2-methyl-4-<(2)H3>methylphenyl>propane

There total 5 articles about 2-cyano-2-(1-ethoxyethoxy)-1-<3,5-bis(benzyloxy)-2-methyl-4-<(2)H3>methylphenyl>propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-44-7
benzyl chloride

: 89505-66-8
2-cyano-2-(1-ethoxyethoxy)-1-<3,5-bis(benzyloxy)-2-methyl-4-<(2)H3>methylphenyl>propane

Guidance literature:: Multi-step reaction with 4 steps

1: 63 percent / potassium carbonate / butan-2-one / 6 h / Heating

2: 77 percent / lithium aluminium hydride / tetrahydrofuran / 0.25 h

3: 81 percent / phosphorous tribromide / diethyl ether / 0.08 h

4: 1.) lithium di-isopropylamide / 1.) THF, -78 deg C, 5 min, 2.) 1 h

With lithium aluminium tetrahydride; phosphorus tribromide; potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; butanone;

Reference yield:

: 89505-61-3
3,5-dihydroxy-2-methyl-4-<(2)H3>methylbenzoic acid

: 89505-66-8
2-cyano-2-(1-ethoxyethoxy)-1-<3,5-bis(benzyloxy)-2-methyl-4-<(2)H3>methylphenyl>propane

Guidance literature:: Multi-step reaction with 5 steps

1: 75 percent / diethyl ether / 0 °C

2: 63 percent / potassium carbonate / butan-2-one / 6 h / Heating

3: 77 percent / lithium aluminium hydride / tetrahydrofuran / 0.25 h

4: 81 percent / phosphorous tribromide / diethyl ether / 0.08 h

5: 1.) lithium di-isopropylamide / 1.) THF, -78 deg C, 5 min, 2.) 1 h

With lithium aluminium tetrahydride; phosphorus tribromide; potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; butanone;

Reference yield:

: 89505-64-6
3,5-bis(benzyloxy)-2-methyl-4-<(2)H3>methylbenzyl alcohol

: 89505-66-8
2-cyano-2-(1-ethoxyethoxy)-1-<3,5-bis(benzyloxy)-2-methyl-4-<(2)H3>methylphenyl>propane

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / phosphorous tribromide / diethyl ether / 0.08 h

2: 1.) lithium di-isopropylamide / 1.) THF, -78 deg C, 5 min, 2.) 1 h

With phosphorus tribromide; lithium diisopropyl amide; In diethyl ether;