trans-1,2-biscyclobutane

Base Information

Chemical Name:trans-1,2-biscyclobutane
CAS No.:55980-59-1
Molecular Formula:C₂₀H₂₆N₂
Molecular Weight:294.44
Hs Code.:

trans-1,2-bis<p-(dimethylamino)phenyl>cyclobutane

Synonyms:trans-1,2-biscyclobutane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-1,2-biscyclobutane

Chemical Property:

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Technology Process of trans-1,2-biscyclobutane

There total 3 articles about trans-1,2-biscyclobutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 2039-80-7
N,N-dimethy-4-vinylaniline

: 55980-59-1
trans-1,2-biscyclobutane

Guidance literature:: With ferric nitrate; In methanol; for 1.5h; Ambient temperature;
DOI:10.1021/jo01293a015

Reference yield:

: 5338-94-3
1-[4-(N,N-dimethylamino)phenyl]ethanol

: 55980-59-1
trans-1,2-biscyclobutane

Guidance literature:: Multi-step reaction with 2 steps

1: flash distillation at 150 deg C under vacuum

2: 81 percent / Fe(NO₃)3 / methanol / 1.5 h / Ambient temperature

With ferric nitrate; In methanol;
DOI:10.1021/jo01293a015

Reference yield:

: 100-10-7
4-dimethylamino-benzaldehyde

: 55980-59-1
trans-1,2-biscyclobutane

Guidance literature:: Multi-step reaction with 3 steps

1: 1) Mg / 1) diethyl ether, 1h; 2) diethyl ether, 3h

2: flash distillation at 150 deg C under vacuum

3: 81 percent / Fe(NO₃)3 / methanol / 1.5 h / Ambient temperature

With magnesium; ferric nitrate; In methanol;
DOI:10.1021/jo01293a015