Boc-PheΨGly-ACHPA-Leu-NHCH2-m-Ph-CH2NH2

Base Information

Chemical Name:Boc-PheΨGly-ACHPA-Leu-NHCH2-m-Ph-CH2NH2
CAS No.:124338-93-8
Molecular Formula:C₄₂H₆₅N₅O₆
Molecular Weight:736.008
Hs Code.:

Boc-PheΨ<CH2CH2>Gly-ACHPA-Leu-NHCH2-m-Ph-CH2NH2

Synonyms:Boc-PheΨGly-ACHPA-Leu-NHCH2-m-Ph-CH2NH2

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Boc-PheΨGly-ACHPA-Leu-NHCH2-m-Ph-CH2NH2

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Technology Process of Boc-PheΨGly-ACHPA-Leu-NHCH2-m-Ph-CH2NH2

There total 3 articles about Boc-PheΨGly-ACHPA-Leu-NHCH2-m-Ph-CH2NH2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82001-64-7
(E)-(S)-<1-(phenylmethyl)-5-(trimethylsilyl)-3-hexen-5-ynyl>carbamic acid 1,1-dimethylethyl ester

: 124338-93-8
Boc-PheΨGly-ACHPA-Leu-NHCH2-m-Ph-CH2NH2

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) (cyclohexyl)2BH, 2.) 2 N NaOH, 30percent H₂O₂ / 1.) THF, 0 deg C, 1 h, 2.) MeOH, room temp., 1 h

2: 0.45 g / H₂ / 10percent Pd/C / propan-2-ol / 20 °C / 2637.5 Torr

3: HOBT/DCC, Et₃N / dimethylformamide / 1.) 0 deg C, 0.5 h, 2.) room temp.

With sodium hydroxide; bis(cyclohexanyl)borane; hydrogen; dihydrogen peroxide; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/jm00164a058

Reference yield:

: 82042-48-6
(S)-5-<(tert-Butoxycarbonyl)amino>-6-phenyl-(E)-3-hexenoic acid

: 124338-93-8
Boc-PheΨGly-ACHPA-Leu-NHCH2-m-Ph-CH2NH2

Guidance literature:: Multi-step reaction with 2 steps

1: 0.45 g / H₂ / 10percent Pd/C / propan-2-ol / 20 °C / 2637.5 Torr

2: HOBT/DCC, Et₃N / dimethylformamide / 1.) 0 deg C, 0.5 h, 2.) room temp.

With hydrogen; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/jm00164a058

Reference yield:

: 118387-85-2
Boc-PheΨGly

: 124338-93-8
Boc-PheΨGly-ACHPA-Leu-NHCH2-m-Ph-CH2NH2

Guidance literature:: With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; 1.) 0 deg C, 0.5 h, 2.) room temp.;
DOI:10.1021/jm00164a058