1-[4-(4-methoxyphenylthio)-2,3,5,6-tetrafluorophenylthio]-4-benzoyl-2,3,5,6-tetrafluorobenzene

Base Information

Chemical Name:1-[4-(4-methoxyphenylthio)-2,3,5,6-tetrafluorophenylthio]-4-benzoyl-2,3,5,6-tetrafluorobenzene
CAS No.:1447769-37-0
Molecular Formula:C₂₆H₁₂F₈O₂S₂
Molecular Weight:572.499
Hs Code.:

Synonyms:1-[4-(4-methoxyphenylthio)-2,3,5,6-tetrafluorophenylthio]-4-benzoyl-2,3,5,6-tetrafluorobenzene

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Chemical Property of 1-[4-(4-methoxyphenylthio)-2,3,5,6-tetrafluorophenylthio]-4-benzoyl-2,3,5,6-tetrafluorobenzene

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Technology Process of 1-[4-(4-methoxyphenylthio)-2,3,5,6-tetrafluorophenylthio]-4-benzoyl-2,3,5,6-tetrafluorobenzene

There total 3 articles about 1-[4-(4-methoxyphenylthio)-2,3,5,6-tetrafluorophenylthio]-4-benzoyl-2,3,5,6-tetrafluorobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 57517-98-3
4-(2,3,4,5,6-pentafluorophenylthio)-1-methoxybenzene

: 1402596-62-6
bis(4-benzoyl-2,3,5,6-tetrafluorophenyl) sulfide

: 1447769-37-0
1-[4-(4-methoxyphenylthio)-2,3,5,6-tetrafluorophenylthio]-4-benzoyl-2,3,5,6-tetrafluorobenzene

: 1447769-42-7
bis[4-(4-methoxyphenylthio)-2,3,5,6-tetrafluorophenyl] sulfide

Guidance literature:: With hydridotetakis(triphenylphosphine)rhodium(I); chlorotriisopropylsilane; o-phenylenebis(diphenylphosphine); In tetrahydrofuran; for 6h; Reflux; Inert atmosphere;
DOI:10.1016/j.tetlet.2013.06.021

Reference yield:

: 1536-23-8
2,3,4,5,6-pentafluorobenzophenone

: 1447769-37-0
1-[4-(4-methoxyphenylthio)-2,3,5,6-tetrafluorophenylthio]-4-benzoyl-2,3,5,6-tetrafluorobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: hydridotetakis(triphenylphosphine)rhodium(I); o-phenylenebis(diphenylphosphine); chlorotriisopropylsilane / tetrahydrofuran / 6 h / Reflux; Inert atmosphere

2: hydridotetakis(triphenylphosphine)rhodium(I); o-phenylenebis(diphenylphosphine); chlorotriisopropylsilane / tetrahydrofuran / 6 h / Reflux; Inert atmosphere

With hydridotetakis(triphenylphosphine)rhodium(I); chlorotriisopropylsilane; o-phenylenebis(diphenylphosphine); In tetrahydrofuran;
DOI:10.1016/j.tetlet.2013.06.021

Reference yield:

: 1402596-61-5
1-(4-phenylthio-2,3,5,6-tetrafluorophenylthio)-4-benzoyl-2,3,5,6-tetrafluorobenzene

: 1447769-37-0
1-[4-(4-methoxyphenylthio)-2,3,5,6-tetrafluorophenylthio]-4-benzoyl-2,3,5,6-tetrafluorobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: hydridotetakis(triphenylphosphine)rhodium(I); o-phenylenebis(diphenylphosphine) / chlorobenzene / 12 h / Inert atmosphere; Reflux

2: hydridotetakis(triphenylphosphine)rhodium(I); o-phenylenebis(diphenylphosphine); chlorotriisopropylsilane / tetrahydrofuran / 6 h / Reflux; Inert atmosphere

With hydridotetakis(triphenylphosphine)rhodium(I); chlorotriisopropylsilane; o-phenylenebis(diphenylphosphine); In tetrahydrofuran; chlorobenzene;
DOI:10.1016/j.tetlet.2013.06.021