Dimethyl-dithiocarbamic acid 2-acenaphthen-5-yl-2-oxo-1-phenyl-ethyl ester

Base Information

Chemical Name:Dimethyl-dithiocarbamic acid 2-acenaphthen-5-yl-2-oxo-1-phenyl-ethyl ester
CAS No.:180746-56-9
Molecular Formula:C₂₃H₂₁NOS₂
Molecular Weight:391.558
Hs Code.:

Synonyms:Dimethyl-dithiocarbamic acid 2-acenaphthen-5-yl-2-oxo-1-phenyl-ethyl ester

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Chemical Property of Dimethyl-dithiocarbamic acid 2-acenaphthen-5-yl-2-oxo-1-phenyl-ethyl ester

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Technology Process of Dimethyl-dithiocarbamic acid 2-acenaphthen-5-yl-2-oxo-1-phenyl-ethyl ester

There total 1 articles about Dimethyl-dithiocarbamic acid 2-acenaphthen-5-yl-2-oxo-1-phenyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 681463-28-5
1-acenaphthen-5-yl-2-bromo-2-phenyl-ethanone

: 598-64-1
dimethylammonium dimethyldithiocarbamate

: 180746-56-9
Dimethyl-dithiocarbamic acid 2-acenaphthen-5-yl-2-oxo-1-phenyl-ethyl ester

Guidance literature:: In 1,4-dioxane; methanol; at 60 ℃; for 0.5h;

Reference yield: 84.0%

: 180746-56-9
Dimethyl-dithiocarbamic acid 2-acenaphthen-5-yl-2-oxo-1-phenyl-ethyl ester

: 2-(N,N-Dimethylamino)-4-acenaphthen-5-yl-5-phenyl-1,3-dithioliumperchlorat

Guidance literature:: With perchloric acid; for 0.333333h; Heating;

Reference yield:

: 180746-56-9
Dimethyl-dithiocarbamic acid 2-acenaphthen-5-yl-2-oxo-1-phenyl-ethyl ester

: (Z)-5,5'-Di-acenaphthen-5-yl-4,4'-diphenyl-[2,2']bi[[1,3]dithiolylidene]

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / 70percent HClO₄ / 0.33 h / Heating

2: 91 percent / pyridine, H₂S / acetonitrile / 0.75 h

3: 0.25 h / 140 - 150 °C

4: 30 percent / PPh₃ / acetonitrile / 3 h / 20 °C

With pyridine; perchloric acid; hydrogen sulfide; triphenylphosphine; In acetonitrile;