benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteinyl-L-prolyl-L-leucyl-glycine amide

Base Information

Chemical Name:benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteinyl-L-prolyl-L-leucyl-glycine amide
CAS No.:78221-61-1
Molecular Formula:C₃₄H₄₇N₅O₆S
Molecular Weight:653.843
Hs Code.:

Synonyms:benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteinyl-L-prolyl-L-leucyl-glycine amide

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Chemical Property of benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteinyl-L-prolyl-L-leucyl-glycine amide

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Technology Process of benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteinyl-L-prolyl-L-leucyl-glycine amide

There total 3 articles about benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteinyl-L-prolyl-L-leucyl-glycine amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 2002-44-0
melanostatin

: 78221-56-4
N-benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteine

: 78221-61-1
benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteinyl-L-prolyl-L-leucyl-glycine amide

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; 1) 0 deg C, 1 h; 2) room temp., 20 h;
DOI:10.1135/cccc19810286

Reference yield:

: 78221-55-3
S-(2,4,6-trimethylbenzyl)-L-cysteine

: 78221-61-1
benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteinyl-L-prolyl-L-leucyl-glycine amide

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / NaOH / H₂O / 0.5 h / Ambient temperature

2: 86 percent / dicyclohexylcarbodiimide, hydroxybenzotriazole / dimethylformamide / 1) 0 deg C, 1 h; 2) room temp., 20 h

With sodium hydroxide; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In water; N,N-dimethyl-formamide;
DOI:10.1135/cccc19810286

Reference yield:

: 1585-16-6
2-chloromethyl-1,3,5-trimethylbenzene

: 78221-61-1
benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteinyl-L-prolyl-L-leucyl-glycine amide

Guidance literature:: Multi-step reaction with 3 steps

1: 1) Na, liquid NH₃ / 1) 15 min; 2) 2 h

2: 69 percent / NaOH / H₂O / 0.5 h / Ambient temperature

3: 86 percent / dicyclohexylcarbodiimide, hydroxybenzotriazole / dimethylformamide / 1) 0 deg C, 1 h; 2) room temp., 20 h

With sodium hydroxide; ammonia; sodium; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In water; N,N-dimethyl-formamide;
DOI:10.1135/cccc19810286