5,15-Bis(3,5-di-tert-butylphenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin

Base Information

Chemical Name:5,15-Bis(3,5-di-tert-butylphenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin
CAS No.:138253-31-3
Molecular Formula:C₆₀H₇₈N₄
Molecular Weight:855.306
Hs Code.:

Synonyms:5,15-Bis(3,5-di-tert-butylphenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin

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Chemical Property of 5,15-Bis(3,5-di-tert-butylphenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin

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Technology Process of 5,15-Bis(3,5-di-tert-butylphenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin

There total 8 articles about 5,15-Bis(3,5-di-tert-butylphenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 92415-30-0
bis(3-ethyl-4-methyl-1H-pyrrol-2-yl)methane

: 17610-00-3
3,5-Di-tert-butylbenzaldehyde

: 138253-30-2
4'-(4-formylphenyl)-[2,2':6',2'']terpyridine

: 138253-31-3
5,15-Bis(3,5-di-tert-butylphenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin

: 138253-32-4
(1Z,4Z,9Z,15Z)-5-(3,5-Di-tert-butyl-phenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethyl-15-(4-[2,2';6',2'']terpyridin-4'-yl-phenyl)-porphyrin

: 138253-33-5
5,15-bis<4-(4'-phenyl-2,2':6',2''-terpyridinyl)>-3,7,13,17-tetraethyl-2,8,12,18-tetramethylporphyrin

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 15h; Ambient temperature;
DOI:10.1016/S0040-4039(00)79442-1

Reference yield: 22.0%

: 872-85-5
pyridine-4-carbaldehyde

: 92415-30-0
bis(3-ethyl-4-methyl-1H-pyrrol-2-yl)methane

: 17610-00-3
3,5-Di-tert-butylbenzaldehyde

: C₅₁H₆₁N₅

: 123747-40-0
2,8,12,18-tetraethyl-3,7,13,17-tetramethyl-5,15-bis(pyridin-4-yl)porphyrin

: 138253-31-3
5,15-Bis(3,5-di-tert-butylphenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin

Guidance literature:: pyridine-4-carbaldehyde; bis(3-ethyl-4-methyl-1H-pyrrol-2-yl)methane; 3,5-Di-tert-butylbenzaldehyde; With chloroacetic acid; In dichloromethane; at 20 ℃; for 4h; Darkness; Inert atmosphere;

With chloranil; In tetrahydrofuran; dichloromethane;
DOI:10.1134/S1070363217120556

Reference yield:

: 92415-30-0
bis(3-ethyl-4-methyl-1H-pyrrol-2-yl)methane

: 17610-00-3
3,5-Di-tert-butylbenzaldehyde

: 77123-57-0
4-[(trimethylsilyl)ethynyl]bezaldehyde

: 138253-31-3
5,15-Bis(3,5-di-tert-butylphenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin

: 5-(3,5-Di-tert-butylphenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethyl-15-{4-[(trimethylsilyl)ethynyl]phenyl}porphyrin

Guidance literature:: bis(3-ethyl-4-methyl-1H-pyrrol-2-yl)methane; 3,5-Di-tert-butylbenzaldehyde; 4-[(trimethylsilyl)ethynyl]bezaldehyde; With trichloroacetic acid; In acetonitrile; at 20 ℃; for 18h;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; acetonitrile; at 20 ℃; for 3h;
DOI:10.1055/s-1999-3525