N-(2,6-dimethylphenyl)-2,5-dihydro-2-imino-4,5,5-trimethylfuran-3-carboxamide hydrogensulfate

Base Information

Chemical Name:N-(2,6-dimethylphenyl)-2,5-dihydro-2-imino-4,5,5-trimethylfuran-3-carboxamide hydrogensulfate
CAS No.:1370047-95-2
Molecular Formula:C₁₆H₂₀N₂O₂*H₂O₄S
Molecular Weight:370.426
Hs Code.:

Synonyms:N-(2,6-dimethylphenyl)-2,5-dihydro-2-imino-4,5,5-trimethylfuran-3-carboxamide hydrogensulfate

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Chemical Property of N-(2,6-dimethylphenyl)-2,5-dihydro-2-imino-4,5,5-trimethylfuran-3-carboxamide hydrogensulfate

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Technology Process of N-(2,6-dimethylphenyl)-2,5-dihydro-2-imino-4,5,5-trimethylfuran-3-carboxamide hydrogensulfate

There total 3 articles about N-(2,6-dimethylphenyl)-2,5-dihydro-2-imino-4,5,5-trimethylfuran-3-carboxamide hydrogensulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1370047-82-7
N-(2,6-dimethylphenyl)-2,5-dihydro-2-imino-4,5,5-trimethylfuran-3-carboxamide

: 1370047-95-2
N-(2,6-dimethylphenyl)-2,5-dihydro-2-imino-4,5,5-trimethylfuran-3-carboxamide hydrogensulfate

Guidance literature:: With sulfuric acid; In ethanol; water; at 20 ℃; for 0.166667h;
DOI:10.1007/s00706-011-0615-2

Reference yield:

: 1370047-90-7
N-(2,6-dimethylphenyl)-2,5-dihydro-2-imino-4,5,5-trimethylfuran-3-carboxamide hydrochloride

: 1370047-95-2
N-(2,6-dimethylphenyl)-2,5-dihydro-2-imino-4,5,5-trimethylfuran-3-carboxamide hydrogensulfate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; sodium hydroxide / water / pH 7 - 8

2: sulfuric acid / ethanol; water / 0.17 h / 20 °C

With sulfuric acid; potassium carbonate; sodium hydroxide; In ethanol; water;
DOI:10.1007/s00706-011-0615-2

Reference yield:

: 115-22-0
3-Hydroxy-3-methyl-2-butanone

: 1370047-95-2
N-(2,6-dimethylphenyl)-2,5-dihydro-2-imino-4,5,5-trimethylfuran-3-carboxamide hydrogensulfate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium methylate / methanol / 5 h / 35 - 40 °C

2: sulfuric acid / ethanol; water / 0.17 h / 20 °C

With sulfuric acid; sodium methylate; In methanol; ethanol; water;
DOI:10.1007/s00706-011-0615-2