N'-(3-cyano-4,5-diphenyl-2-thienyl)-N,N-dimethylethanimidamide

Base Information

• Chemical Name: N'-(3-cyano-4,5-diphenyl-2-thienyl)-N,N-dimethylethanimidamide
• CAS No.: 1179316-54-1
• Molecular Formula: C₂₁H₁₉N₃S
• Molecular Weight: 345.468
• Mol file: 1179316-54-1.mol

Synonyms:N'-(3-cyano-4,5-diphenyl-2-thienyl)-N,N-dimethylethanimidamide

Chemical Property of N'-(3-cyano-4,5-diphenyl-2-thienyl)-N,N-dimethylethanimidamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of N'-(3-cyano-4,5-diphenyl-2-thienyl)-N,N-dimethylethanimidamide

There total 1 articles about N'-(3-cyano-4,5-diphenyl-2-thienyl)-N,N-dimethylethanimidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

N,N-dimethylacetamide dimethyl acetal (18871-66-4) + 2-amino-4,5-diphenylthiophene-3-carbonitrile (42160-34-9) → N'-(3-cyano-4,5-diphenyl-2-thienyl)-N,N-dimethylethanimidamide (1179316-54-1)

Guidance literature:

In methanol; for 5h; Reflux;

DOI:10.1016/j.bmc.2009.05.016

Reference yield: 96.0%

N'-(3-cyano-4,5-diphenyl-2-thienyl)-N,N-dimethylethanimidamide (1179316-54-1) → N6,N6-dimethyl-2,3-diphenylthieno[2,3-b]pyridine-4,6-diamine (1179316-59-6)

Guidance literature:

With sodium amide; In toluene; at 50 ℃; for 5h; Reflux; Inert atmosphere;

DOI:10.1016/j.bmc.2009.05.016

upstream raw materials:

N,N-dimethylacetamide dimethyl acetal

2-amino-4,5-diphenylthiophene-3-carbonitrile

Downstream raw materials:

N₆,N₆-dimethyl-2,3-diphenylthieno[2,3-b]pyridine-4,6-diamine