Technology Process of C19H23NO2
There total 6 articles about C19H23NO2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C18H23NO;
With
potassium hexamethylsilazane;
In
tetrahydrofuran; toluene;
at -78 ℃;
for 0.25h;
Inert atmosphere;
2,2,2-trifluoroethyl formate;
In
tetrahydrofuran; toluene;
for 1h;
Inert atmosphere;
With
ammonium chloride;
In
tetrahydrofuran; water; toluene;
Saturated solution;
DOI:10.1021/ol201122f
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium hydroxide / ethanol / 4 h / 80 °C / Inert atmosphere
1.2: 20 °C / Saturated solution
2.1: tetra(n-butyl)ammonium hydroxide / water; toluene / 1.5 h / 50 °C / Inert atmosphere
3.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.25 h / -78 °C / Inert atmosphere
3.2: 1 h / Inert atmosphere
3.3: Saturated solution
With
tetra(n-butyl)ammonium hydroxide; potassium hexamethylsilazane; potassium hydroxide;
In
tetrahydrofuran; ethanol; water; toluene;
DOI:10.1021/ol201122f
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: tetra(n-butyl)ammonium hydroxide / water; toluene / 1.5 h / 50 °C / Inert atmosphere
2.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.25 h / -78 °C / Inert atmosphere
2.2: 1 h / Inert atmosphere
2.3: Saturated solution
With
tetra(n-butyl)ammonium hydroxide; potassium hexamethylsilazane;
In
tetrahydrofuran; water; toluene;
DOI:10.1021/ol201122f
