3,3'-<(1-Methylethylidene)bis(4,1-phenyleneoxy)>bis(2-chloro-2,3,3-trifluoropropanol)

Base Information

Chemical Name:3,3'-<(1-Methylethylidene)bis(4,1-phenyleneoxy)>bis(2-chloro-2,3,3-trifluoropropanol)
CAS No.:131043-07-7
Molecular Formula:C₂₁H₂₀Cl₂F₆O₄
Molecular Weight:521.284
Hs Code.:

Synonyms:3,3'-<(1-Methylethylidene)bis(4,1-phenyleneoxy)>bis(2-chloro-2,3,3-trifluoropropanol)

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Chemical Property of 3,3'-<(1-Methylethylidene)bis(4,1-phenyleneoxy)>bis(2-chloro-2,3,3-trifluoropropanol)

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Technology Process of 3,3'-<(1-Methylethylidene)bis(4,1-phenyleneoxy)>bis(2-chloro-2,3,3-trifluoropropanol)

There total 2 articles about 3,3'-<(1-Methylethylidene)bis(4,1-phenyleneoxy)>bis(2-chloro-2,3,3-trifluoropropanol) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 131043-06-6
Dimethyl 3,3'-<(1-methylethylidene)bis(4,1-phenyleneoxy)>bis(2-chloro-2,3,3-trifluoropropionate)

: 131043-07-7
3,3'-<(1-Methylethylidene)bis(4,1-phenyleneoxy)>bis(2-chloro-2,3,3-trifluoropropanol)

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 0.5h;
DOI:10.1021/jo00001a030

Reference yield:

: 2444-90-8,17224-35-0,53794-62-0
bisphenol A disodium salt

: 131043-07-7
3,3'-<(1-Methylethylidene)bis(4,1-phenyleneoxy)>bis(2-chloro-2,3,3-trifluoropropanol)

Guidance literature:: Multi-step reaction with 2 steps

1: 1) DMSO, 25 deg C, 190 psi, several hours 2) r.t.

2: 74 percent / LiAlH₄ / tetrahydrofuran / 0.5 h

With lithium aluminium tetrahydride; In tetrahydrofuran;
DOI:10.1021/jo00001a030