[3-(1R,3S)-benzyloxycarbonylaminocyclohexyl]-1-carbamic acid tertbutyl ester

Base Information

Chemical Name:[3-(1R,3S)-benzyloxycarbonylaminocyclohexyl]-1-carbamic acid tertbutyl ester
CAS No.:1261225-49-3
Molecular Formula:C₁₉H₂₈N₂O₄
Molecular Weight:348.442
Hs Code.:

Synonyms:[3-(1R,3S)-benzyloxycarbonylaminocyclohexyl]-1-carbamic acid tertbutyl ester

Suppliers and Price of [3-(1R,3S)-benzyloxycarbonylaminocyclohexyl]-1-carbamic acid tertbutyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of [3-(1R,3S)-benzyloxycarbonylaminocyclohexyl]-1-carbamic acid tertbutyl ester

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of [3-(1R,3S)-benzyloxycarbonylaminocyclohexyl]-1-carbamic acid tertbutyl ester

There total 26 articles about [3-(1R,3S)-benzyloxycarbonylaminocyclohexyl]-1-carbamic acid tertbutyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1259278-11-9
benzyl N-[(1S,3R)-3-carbamoylcyclohexyl]carbamate

: 1907-33-1
lithium tert-butoxide

: 1261225-49-3
[3-(1R,3S)-benzyloxycarbonylaminocyclohexyl]-1-carbamic acid tertbutyl ester

Guidance literature:: With copper(ll) bromide; In tetrahydrofuran;
DOI:10.1021/acs.oprd.6b00063

Reference yield: 86.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1259278-12-0,1223158-00-6,1261225-45-9
benzyl N-[(1S,3R)-3-aminocyclohexyl]carbamate

: 1261225-49-3
[3-(1R,3S)-benzyloxycarbonylaminocyclohexyl]-1-carbamic acid tertbutyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 15 ℃; for 12h;

Reference yield: 79.0%

: (1S,3R)-3-(tert-butoxycarbonylamino)cyclohexanecarboxylic acid

: 100-51-6,185532-71-2
benzyl alcohol

: 1261225-49-3
[3-(1R,3S)-benzyloxycarbonylaminocyclohexyl]-1-carbamic acid tertbutyl ester

Guidance literature:: (1S,3R)-3-(tert-butoxycarbonylamino)cyclohexanecarboxylic acid; With diphenyl phosphoryl azide; triethylamine; In toluene; at 110 ℃; for 2h;

benzyl alcohol; In toluene; at 80 ℃; for 2h;